Heat-insulating thermal-insulating 3D printing material and preparation method thereof
A 3D printing, thermal insulation technology, applied in the field of 3D printing materials, can solve problems such as poor thermal insulation effect, poor bacteriostatic effect, and toxic gas discharge, and achieve the effect of good thermal insulation effect, good antibacterial effect, and safe use.
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Embodiment 1
[0027] A thermal insulation 3D printing material, the 3D printing material includes the following raw materials in parts by weight: 55 parts of polylactic acid, 18 parts of melamine resin powder, 13 parts of triphenylphosphine, 5 parts of acetylglutamine, polyamino poly 6 parts of ether-based methylene phosphonic acid, 5 parts of water-soluble thiosulfate, and 2 parts of nickel nitrate. The water-soluble thiosulfate salt is lithium thiosulfate.
[0028] A method for preparing a heat-insulating 3D printing material, comprising the following steps: (1) mixing acetylglutamine and water-soluble thiosulfate, adding water twice the mass of the mixture, and mixing uniformly to obtain a mixture 1; ( 2) Mix nickel nitrate with 0.5 times the mass of water, stir evenly to obtain a nickel nitrate solution; (3) mix triphenylphosphine with 70% ethanol solution with 1 mass of its mass, and stir uniformly to obtain mixture 2; (4) ) Mix mixture 1 with polyamino polyether methylene phosphonic ...
Embodiment 2
[0030] A thermal insulation 3D printing material, the 3D printing material includes the following raw materials in parts by weight: 80 parts of polylactic acid, 30 parts of melamine resin powder, 16 parts of triphenylphosphine, 11 parts of acetylglutamine, polyamino poly 11 parts of ether-based methylene phosphonic acid, 10 parts of water-soluble thiosulfate, and 5 parts of nickel nitrate. The water soluble thiosulfate is sodium thiosulfate.
[0031] A method for preparing a heat-insulating 3D printing material, comprising the following steps: (1) mixing acetylglutamine and water-soluble thiosulfate, adding water 4 times the mass of the mixture, and mixing uniformly to obtain a mixture 1; ( 2) Mix nickel nitrate with 1 times the mass of water, stir evenly to obtain nickel nitrate solution; (3) mix triphenylphosphine with 70% ethanol solution with 2 times the mass, stir uniformly to obtain mixture 2; (4) ) Mix mixture 1 with polyamino polyether methylene phosphonic acid, stir ...
Embodiment 3
[0033] A thermal insulation 3D printing material, the 3D printing material includes the following raw materials in parts by weight: 68 parts of polylactic acid, 25 parts of melamine resin powder, 15 parts of triphenylphosphine, 9 parts of acetylglutamine, polyamino poly 8 parts of ether-based methylene phosphonic acid, 6 parts of water-soluble thiosulfate, and 4 parts of nickel nitrate. The water soluble thiosulfate is potassium thiosulfate.
[0034] A method for preparing a heat-insulating 3D printing material, comprising the following steps: (1) mixing acetylglutamine and water-soluble thiosulfate, adding water three times the mass of the mixture, and mixing uniformly to obtain a mixture one. (2) Mix the nickel nitrate with 0.7 times the mass of water, and stir evenly to obtain a nickel nitrate solution. (3) Mix triphenylphosphine with its 1.6 times mass of 70% ethanol solution and stir evenly to obtain mixture 2. (4) Mix mixture 1 and polyaminopolyether methylene phosphon...
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