Method for recycling phosphorus from sludge ash
A cyclic extraction and sludge ash technology, applied in chemical instruments and methods, phosphorus compounds, inorganic chemistry, etc., can solve the problems of low phosphorus extraction rate, a large amount of waste liquid, and large consumption of chemicals, so as to reduce the difficulty of extraction and avoid Pollution, the effect of favoring the precipitation of phosphorus
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Embodiment 1
[0033] A method for circularly extracting phosphorus from sludge ash, comprising the following steps:
[0034] (1) Get the sludge incineration ash in the urban domestic sewage treatment plant, and pass through a 100-mesh sieve after ball milling;
[0035] (2) heating the sulfuric acid solution with a mass fraction of 10% to 25° C., and then mixing it with sludge ash at a liquid-solid ratio of 3 mL / g to obtain a slurry;
[0036] (3) Put the slurry in a stirring container, stir and react at 25°C and 150rmp for 30 minutes, then add deionized water to terminate the reaction, then perform suction filtration on the reacted slurry, and filter the sludge after suction filtration The cake is washed with distilled water, and the cleaning liquid and the filtrate are combined to obtain an extract;
[0037] (4) the sulfuric acid solution that is 98% by extracting solution and mass fraction is mixed by the volume ratio of 28.8:1.2, prepares extractant, replaces the sulfuric acid solution i...
Embodiment 2
[0040] A method for circularly extracting phosphorus from sludge ash, comprising the following steps:
[0041] (1) Get the sludge incineration ash in the urban domestic sewage treatment plant, and pass through a 100-mesh sieve after ball milling;
[0042] (2) Heating the sulfuric acid solution with a mass fraction of 7% to 45° C., and then mixing it with sludge ash at a liquid-solid ratio of 4 mL / g to obtain a slurry;
[0043] (3) Put the slurry in a stirring container, stir and react at 45°C and 200rmp for 30 minutes, then add deionized water to terminate the reaction, then perform suction filtration on the reacted slurry, and filter the sludge after suction filtration The cake is washed with distilled water, and the cleaning liquid and the filtrate are combined to obtain an extract;
[0044] (4) the sulfuric acid solution that is 98% by extracting solution and mass fraction is mixed by the volume ratio of 28.4:1.2, prepares extractant, replaces the sulfuric acid solution in...
Embodiment 3
[0047] A method for circularly extracting phosphorus from sludge ash, comprising the following steps:
[0048] (1) Get the sludge incineration ash in the urban domestic sewage treatment plant, and pass through a 100-mesh sieve after ball milling;
[0049](2) heating the sulfuric acid solution with a mass fraction of 13% to 30° C., and then mixing it with sludge ash at a liquid-solid ratio of 5 mL / g to obtain a slurry;
[0050] (3) Put the slurry in a stirring container, stir and react at 30°C and 300rmp for 30 minutes, then add deionized water to terminate the reaction, then perform suction filtration on the reacted slurry, and filter the sludge after suction filtration The cake is washed with distilled water, and the cleaning liquid and the filtrate are combined to obtain an extract;
[0051] (4) the sulfuric acid solution that extracting solution and mass fraction are 13% is mixed by the volume ratio of 28.4:1.6, prepares extractant, replaces the sulfuric acid solution in s...
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