Preparation method of Ni2P2O7 film
A thin film and electrolyte technology, applied in the field of Ni2P2O7 thin film preparation, can solve the problems of lack of thin film preparation methods and less research, and achieve the effect of good surface smoothness and good surface density
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0029] Example 1:
[0030] A kind of Ni 2 P 2 O 7 The preparation method of the film adopts standard three-electrode cyclic voltammetry to deposit on the ITO surface,
[0031] The electrolyte and concentration of the electrolyte used are: 0.1mmol / L NaH 2 PO 2 , 0.2mmol / L of C 6 H 5 Na 3 O 7 And 5mmol / L NiSO 4 ;
[0032] Among them, platinum sheets and silver / silver chloride (Ag / AgCl) electrodes are used as counter and reference electrodes;
[0033] The deposition process is carried out in the range of -1~0V, the temperature of the electrolyte is 42℃, and the scanning speed is 20 mVs -1 . The scan cycle is 15r.
Example Embodiment
[0034] Example 2:
[0035] A kind of Ni 2 P 2 O 7 The preparation method of the film adopts standard three-electrode cyclic voltammetry to deposit on the ITO surface,
[0036] The electrolyte and concentration of the electrolyte used are: 0.5mmol / L NaH 2 PO 2 , 0.1 mmol / L of C 6 H 5 Na 3 O 7 And 0.2 mmol / L NiSO 4 ;
[0037] Among them, platinum sheets and silver / silver chloride (Ag / AgCl) electrodes are used as counter and reference electrodes;
[0038] The deposition process is carried out in the range of -1.5~0V, the temperature of the electrolyte is 48℃, and the scanning speed is 20 mVs -1 . The scan cycle is 20r.
Example Embodiment
[0039] Example 3:
[0040] A kind of Ni 2 P 2 O 7 The preparation method of the film adopts standard three-electrode cyclic voltammetry to deposit on the ITO surface,
[0041] The electrolyte and concentration of the electrolyte used are: 0.2mmol / L NaH 2 PO 2 , 0.5mmol / L of C 6 H 5 Na 3 O 7 And 1mmol / L NiSO 4 ;
[0042] Among them, platinum sheets and silver / silver chloride (Ag / AgCl) electrodes are used as counter and reference electrodes;
[0043] The deposition process is carried out in the range of -0.5~0V, the temperature of the electrolyte is 45℃, and the scanning speed is 20 mVs -1 . The scan cycle is 25r.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2023 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap