Preparation method of granular urea applicable to paddy rice top application and containing humic acid synergistic carrier
A granular urea and humic acid technology, applied in urea compound fertilizer, nitrogen fertilizer, magnesium fertilizer, etc., can solve the problem of no humic acid urea
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Embodiment 1
[0072] Example 1: Preparation of granular urea containing humic acid synergistic carrier suitable for rice topdressing
[0073] The implementation steps of this embodiment are as follows:
[0074] A, preparation of humic acid extractant
[0075] Add 4 parts by weight of potassium salicylate and 3.0 parts by weight of dimethylformamide to 200 parts by weight of water at a temperature of 64°C, stir and dissolve at 180 rpm, and cool the obtained solution to a temperature below 40°C to obtain the humic acid extractant;
[0076] B, preparation of humic acid extract
[0077] Add 100 parts by weight of weathered coal humic acid mineral raw material with a particle size of 150 meshes to 1000 parts by weight of the humic acid extractant obtained in step A, then gradually raise its temperature to 90°C under stirring, and keep it at this temperature for 54min , then cooled to room temperature, centrifuged at 1000rpm for 50min, and the precipitate was discarded to obtain the humic acid...
Embodiment 2
[0084] Example 2: Preparation of Granular Urea Containing Humic Acid Synergistic Carrier Suitable for Rice Topdressing
[0085] The implementation steps of this embodiment are as follows:
[0086] A, preparation of humic acid extractant
[0087] Add 5 parts by weight of potassium salicylate and 2.4 parts by weight of dimethylformamide to 140 parts by weight of water at a temperature of 70°C, stir and dissolve at 60 rpm, and cool the obtained solution to a temperature below 40°C to obtain the humic acid extractant;
[0088] B, preparation of humic acid extract
[0089] Add 100 parts by weight of lignite humic acid mineral raw material with a particle size of 300 meshes to 1500 parts by weight of the humic acid extractant obtained in step A, then gradually raise its temperature to 90°C under stirring, and keep it at this temperature for 40min, Then cooled to room temperature, centrifuged at 3500rpm for 24min, and the precipitate was discarded to obtain the humic acid extract;...
Embodiment 3
[0096] Example 3: Preparation of granular urea containing humic acid synergistic carrier suitable for rice topdressing
[0097] The implementation steps of this embodiment are as follows:
[0098] A, preparation of humic acid extractant
[0099] Add 2 parts by weight of potassium salicylate and 1.6 parts by weight of dimethylformamide to 170 parts by weight of water at a temperature of 60°C, stir and dissolve at 120 rpm, and cool the obtained solution to a temperature below 40°C to obtain the humic acid extractant;
[0100] B, preparation of humic acid extract
[0101] Add 100 parts by weight of weathered coal humic acid mineral raw material with a particle size of 200 meshes to 1200 parts by weight of the humic acid extractant obtained in step A, then gradually raise its temperature to 90°C under stirring, and keep it at this temperature for 48min , then cooled to room temperature, centrifuged at 1600rpm for 36min, and the precipitate was discarded to obtain the humic acid...
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