Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Novel polyester-cotton disperse dye and reactive dye two-bath dyeing process

A technology of disperse dyes and reactive dyes, which is applied in the field of dyeing, can solve the problems of product quality and enterprise economic benefit decline, wet processing time is long, and has no use value, so as to improve equipment utilization rate and worker production efficiency, and shorten dyeing time , good leveling effect

Inactive Publication Date: 2019-02-01
ANHUI YAYUAN PRINTING & DYEING CO LTD
View PDF4 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The traditional printing and dyeing industry has always adopted the two-bath two-step dyeing method of disperse / reactive dyes for dyeing polyester-cotton blended or interwoven fabrics, that is, dyeing polyester with disperse dyes-reduction cleaning-reactive dyes for over-dyeing cotton. The entire dyeing process takes 10 For several hours, the production efficiency is low, the consumption of water, electricity and steam is large, and the discharge of sewage is large. Moreover, due to the long wet processing time, it is easy to make the cloth surface fluffy and affect the fabric feel, which reduces the product quality and economic benefits of the enterprise.
[0003] The existing disperse / reactive dye one-bath dyeing method replaces the disperse / reactive dye two-bath two-step dyeing method. Although the problems of the two-bath dyeing method can be avoided to a certain extent, there are still many problems in the disperse / reactive dye one-bath dyeing method. Problems, such as the limitations of reactive dyes and disperse dyes used are very large, both reactive dyes and disperse dyes require certain specific dyeing performance requirements, do not have a wide range of use values, and usually cause dye hydrolysis and uneven coloring , resulting in defects such as color flower, color difference, low color fixation rate, etc.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Novel polyester-cotton disperse dye and reactive dye two-bath dyeing process
  • Novel polyester-cotton disperse dye and reactive dye two-bath dyeing process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A novel two-bath dyeing process of polyester-cotton disperse dyes and reactive dyes, comprising the following steps:

[0021] S1, dyeing and washing: immerse the polyester-cotton fabric in the disperse dye microcapsule dye solution, the disperse dye microcapsule dye solution includes: disperse dye microcapsule 1% (owf), pH buffer 3g / L, leveling agent 1g / L, adjust the bath ratio to 1:20, raise the temperature to 130°C at a rate of 2°C / min, keep it for 45 minutes, then cool it down to 70°C at a rate of 2°C / min, keep it for 15 minutes, and after cooling down to room temperature, put it at 50°C Washing with water for 15 minutes and drying at 90°C; the preparation of the disperse dye microcapsules includes: adding β-cyclodextrin to water, then adding citric acid and sodium hypophosphite, β-cyclodextrin, citric acid and hypophosphite The weight ratio of sodium is 12:3:1. After heating up to 100°C, stir and react for 1 hour, cool, filter with suction, and recrystallize with a...

Embodiment 2

[0024] A novel two-bath dyeing process of polyester-cotton disperse dyes and reactive dyes, comprising the following steps:

[0025] S1, dyeing and washing: immerse the polyester-cotton fabric in the disperse dye microcapsule dye solution, the disperse dye microcapsule dye solution includes: disperse dye microcapsule 5% (owf), pH buffer 1g / L, leveling agent 2g / L, adjust the bath ratio to 1:5, heat up to 120°C at a rate of 3°C / min, hold for 55 minutes, then cool down to 80°C at a rate of 1°C / min, hold for 5 minutes, and after cooling down to room temperature, set the temperature at 60°C Washing with water for 5 minutes and drying at 100°C; the preparation of the disperse dye microcapsules includes: adding β-cyclodextrin to water, then adding citric acid and sodium hypophosphite, β-cyclodextrin, citric acid and hypophosphite The weight ratio of sodium is 9:5:1. After heating up to 90°C, stir and react for 2 hours, cool, filter with suction, and recrystallize with a mixed solven...

Embodiment 3

[0028] A novel two-bath dyeing process of polyester-cotton disperse dyes and reactive dyes, comprising the following steps:

[0029]S1, dyeing and washing: immerse the polyester-cotton fabric in the disperse dye microcapsule dye solution, the disperse dye microcapsule dye solution comprises: disperse dye microcapsule 3% (owf), pH buffer 2g / L, leveling agent 1.5 g / L, adjust the bath ratio to 1:15, raise the temperature to 125°C at a rate of 2.5°C / min, keep it for 50 minutes, then cool it down to 75°C at a rate of 1.5°C / min, keep it for 10 minutes, and after cooling down to room temperature, 55°C Wash in water for 10 minutes, and dry at 95°C; the preparation of the disperse dye microcapsules includes: adding β-cyclodextrin to water, then adding citric acid and sodium hypophosphite, β-cyclodextrin, citric acid and hypophosphite The weight ratio of sodium phosphate is 10:4:1. After heating up to 95°C, stir and react for 1.5h, cool, filter with suction, and recrystallize with a mix...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a novel polyester-cotton disperse dye and reactive dye two-bath dyeing process. The method comprises the following steps: S1, dyeing and washing: immersing the polyester cottonfabric into a disperse dye microcapsule dyeing solution, heating the material to 120-130 DEG C, performing insulation for 45 to 55 minutes, cooling the material to 70 to 80 DEG C, performing insulation for 5 to 15 minutes, washing the material with water, and drying the material; and S2, cotton dyeing: immersing the polyester cotton fabric into a finishing solution containing 2,3-epoxypropyltrimethyl ammonium chloride, heating the material to 70-80 DEG C, performing insulation for 50-60 min, and then immersing the material in a reactive dye solution, heating the material to 70-80 DEG C, performing insulation for 10-20min, then adding 5-20g / L of soda ash, performing insulation for 25-35min, and after cooling to room temperature, performing steps of washing, soaping and drying. The noveltwo-bath dyeing process not only has high production efficiency, short process flow, but also uniform coloring and high color fastness.

Description

technical field [0001] The invention relates to the technical field of dyeing, in particular to a novel two-bath dyeing process of polyester-cotton disperse dyes and reactive dyes. Background technique [0002] The traditional printing and dyeing industry has always adopted the two-bath two-step dyeing method of disperse / reactive dyes for dyeing polyester-cotton blended or interwoven fabrics, that is, dyeing polyester with disperse dyes-reduction cleaning-reactive dyes for over-dyeing cotton. The entire dyeing process takes 10 For many hours, the production efficiency is low, the consumption of water, electricity and steam is large, and the amount of sewage discharge is large. Moreover, due to the long wet processing time, it is easy to make the cloth surface fuzzy and affect the fabric feel, which reduces the product quality and economic benefits of the enterprise. [0003] The existing disperse / reactive dye one-bath dyeing method replaces the disperse / reactive dye two-bath...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/38D06P1/16D06P1/44D06P1/66D06P1/673D06P3/872B01J13/02
CPCB01J13/02D06P1/16D06P1/38D06P1/445D06P1/66D06P1/6735D06P3/8252D06P5/002
Inventor 潘学东
Owner ANHUI YAYUAN PRINTING & DYEING CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products