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31results about How to "Whiteness stability" patented technology

Amino-chloro-benzene-containing quaternary ammonium salt type fluorescent whitener, synthesizing method thereof and applications

The invention relates to a series of fluorescent whitening agents containing amino chlorophenyl group quaternary ammonium salt, as well as synthesis and an application of the same. The series of fluorescent whitening agents is mainly applied to papermaking paint printing ink and textile. The synthesis adopts the following steps that: a. cyanuric chloride reacts with amino-chloro-benzene at a temperature between 0 and 5 DEG C for 2.5 h, with pH value controlled to be between 1.8 and 2.1, so as to synthesize one-step condensation product; b. the one-step condensation product reacts with 4, 4'-diaminodiphenylethylene-2, 2'-disulfonic acid at a temperature between 40 and 45 DEG C for 2.5 h, with pH value controlled to be between 3.5 and 4.5, so as to synthesize two-step condensation product; c. the two-step condensation product reacts with a series of tertiary amine compounds at a temperature between 78 and 85 DEG C for 3.0 h, with pH value controlled to be between 7.8 and 8.5, so as to synthesize a series of triazine-DSD acidic fluorescent whitening agents containing amino chlorophenyl group quaternary ammonium salt. Application results show that: the fluorescent whitening agents can be used under neutral/alkaline conditions, and has higher dye uptake rate and better whitening effect under acidic conditions.
Owner:SHANDONG UNIV

Preparation method of phenolic yellowing resistant white chinlon non-ironing fabric

PendingCN112127142AFeel goodDoes not affect the fastness to phenol yellowingLight resistant fibresWrinkle resistant fibresTextile technologyDyeing
The invention belongs to the technical field of textiles, and particularly relates to a preparation method of a phenolic yellowing resistant white chinlon non-ironing fabric. Desizing, pre-tentering,dry shaping, non-ironing, padding, jig dyeing, tentering and pre-shrinking are performed to obtain the fabric, wherein an anti-yellowing finishing agent is added in the pre-tentering process, the non-ironing temperature is 155-165 DEG C, and an anti-phenolic yellowing agent is added in the jig dyeing process. Compared with the conventional white chinlon fabric, the white chinlon non-ironing fabricobtained by the method adopts a high-temperature non-ironing process, has the characteristics of good non-ironing property and washability, and is padded and bleached by using an Ostbook stacking method according to the whiteness requirement, so that the stability of the whiteness of the fabric is improved. The anti-phenolic yellowing agent is added in the jig dyeing process, and a weak cation softener with small influences on yellowing is used for tentering, so that the hand feeling of the fabric is improved, the anti-phenolic yellowing fastness of the fabric is not influenced, the anti-phenolic yellowing fastness of the fabric reaches the grade 4 or above, and the requirement for high quality of high-grade fabrics can be met.
Owner:LUTAI TEXTILE

Pulping process for grinding wood pulp of cotton wood by mechanical abrader

The invention discloses a cotton wood stone ground wood pulping process comprising the following steps of: (1) log sawing and skinning; (2) jordaning with alkali in a wood grinder; (3) screening by a pressure screen; (4) screenings jordaning with alkali in a conical mill; and (5) hydrogen peroxide bleaching. The invention is characterized in that: the wood grinder grindstone of the step (2) adopts bush roll with 4 mesh by primary burring; in the screening process by the pressure slot screen of the step (3), the pulp intake pressure is 0.2-0.4 MPa, the differential pressure is 0.02-0.07 MPa, the pulp intake consistence is 2.5-4.5%, the screenings output volume is 22-35%, the thickness of the screen cut is 0.15-0.35 mm; sodium hydroxide is added in the conical mill of the step (4) to grind screenings, wherein the consumption of the sodium hydroxide is 0.6-0.8% (based on weight percent of oven dry stock), the alkali liquor is added in the pulp intake tank of the conical mill with 40-50 g/l of the alkali liquor concentration, 3.1%-4.54% of jordaning consistency, 0.2-0.3 MPa of jordaning pressure, accordingly, the beating degree of the pulp ground by the conical mill can be increased by 8-12 DEG SR. The pulping process of the invention has advantages of high yield, less pollution, low cost, and the obtained pulp is applicable for paper with various specifications such as pigment offset paper, low weight paper, card paper, color newsprint paper, or the like.
Owner:YUEYANG FOREST & PAPER CO LTD

A kind of preparation technology of vinegar grade bamboo pulp

The invention discloses a preparation process of an acetified bamboo pulp. The process comprises the steps of preparing bamboos, cutting the bamboos, washing the bamboos, pre-hydrolyzing the bamboos, performing soda boiling, washing, screening and bleaching. The steps are characterized in that according to ratio requirements, sinocalamus affinis is more than or equal to 50%, besides, bambusa intermedia and oligostachyum lubricum can be used, and other bamboos can not be used; steam and water are adopted as one of media for pre-hydrolyzing, a sulfate replacement cooking technology is adopted for soda boiling, and an O-D0-EP-D1-Q-P process flow is adopted for bleaching. The yield of the pulp obtained by using the process disclosed by the invention is more than or equal to 32%, the content of alpha cellulose is more than or equal to 96%, the content of pentosan is less than or equal to 5.0%, the degree of polymerization is more than or equal to 800, the whiteness is more than or equal to 88% of ISO (international standardization organization), and the content of an acetone extract is less than or equal to 0.1%, so that the requirements for the acetified bamboo pulp can be met. The preparation process of the acetified bamboo pulp has the characteristics of small corrosion to production equipment, low energy consumption, environmental friendliness, stable quality, safety in production, stability, controllability and low cost, and can easily realize large-scale industrial production.
Owner:泰盛(江西)生活用品有限公司

Method for preparing silver-containing calcium phosphate

The invention discloses a method for preparing silver-containing calcium phosphate and relates to silver-containing calcium phosphate. The method for preparing silver-containing calcium phosphate, disclosed by the invention, is based on a differential reaction technology and has the advantages that the continuous and stable production can be achieved, the process preparation and raw materials are simple, the reaction conditions are mild and controllable, the production cycle is short, and the whiteness is stable. The method comprises the following steps of: (1) preparing raw material liquid; (2) conveying A-phase clear liquid and B-phase clear liquid, which are obtained in the step (1), to a micro-channel continuous mixing system through a pipeline by a metering pump of a raw material conveying system, and carrying out continuous integration reaction so as to form silver-containing calcium phosphate aggregate; (3) conveying a mixing reaction product, namely silver-containing calcium phosphate aggregate sol, to a dehydration and washing device, and drying the washed product so as to obtain amorphous silver-containing calcium phosphate powder; and (4) carrying out high temperature treatment on the amorphous silver-containing calcium phosphate powder obtained in the step (3), thereby obtaining silver-containing calcium phosphate microcrystalline powder with stable whiteness.
Owner:关涛

Pulping process for grinding wood pulp of cotton wood by mechanical abrader

The invention discloses a cotton wood stone ground wood pulping process comprising the following steps of: (1) log sawing and skinning; (2) jordaning with alkali in a wood grinder; (3) screening by a pressure screen; (4) screenings jordaning with alkali in a conical mill; and (5) hydrogen peroxide bleaching. The invention is characterized in that: the wood grinder grindstone of the step (2) adopts bush roll with 4 mesh by primary burring; in the screening process by the pressure slot screen of the step (3), the pulp intake pressure is 0.2-0.4 MPa, the differential pressure is 0.02-0.07 MPa, the pulp intake consistence is 2.5-4.5%, the screenings output volume is 22-35%, the thickness of the screen cut is 0.15-0.35 mm; sodium hydroxide is added in the conical mill of the step (4) to grind screenings, wherein the consumption of the sodium hydroxide is 0.6-0.8% (based on weight percent of oven dry stock), the alkali liquor is added in the pulp intake tank of the conical mill with 40-50 g / l of the alkali liquor concentration, 3.1%-4.54% of jordaning consistency, 0.2-0.3 MPa of jordaning pressure, accordingly, the beating degree of the pulp ground by the conical mill can be increased by 8-12 DEG SR. The pulping process of the invention has advantages of high yield, less pollution, low cost, and the obtained pulp is applicable for paper with various specifications such as pigment offset paper, low weight paper, card paper, color newsprint paper, or the like.
Owner:YUEYANG FOREST & PAPER CO LTD

A kind of production process of white flour kraft cardboard

The invention relates to a production technology of a white top liner. The technology comprises the following steps that 1, ONP pulp is prepared, water is added to fibers obtained from first flotation of the ONP pulp, bleaching is conducted, first ONP pulp is obtained, water is added to fibers obtained from second flotation of the ONP pulp, bleaching is conducted, second ONP pulp is obtained, concentration is conducted on ONP pulp of two times of flotation, and third ONP pulp is conducted; 2, DMOW pulp is conducted, water is added to fibers obtained from first flotation of the DMOW pulp, bleaching is conducted, first DMOW pulp is obtained, water is added to fibers obtained from second flotation of the DMOW pulp, bleaching is conducted, second DMOW pulp is obtained, concentration is conducted on DMOW pulp of two times of flotation, and third DMOW pulp is conducted; 3, the first DMOW pulp, the first ONP pulp and original wood pulp are mixed, a surface layer is obtained after the mixture flows to paper-making meshes, the second DMOW pulp and the second ONP pulp are mixed, a bottom layer is obtained after the mixture flows to the paper-making meshes, the third DMOW pulp, the third ONP pulp and OCC pulp are mixed, and a core layer is obtained after the mixture flows to the paper-making meshes.
Owner:JIANGSU LEE & MAN PAPER MFG
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