Amphipathic alginate with response to light and pH and stable pickering emulsion thereof
An alginate and emulsion technology, applied in the field of pickering emulsions, achieves the effects of large preparation throughput, easy to scale up production, and avoiding operation steps
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[0036] Referring to the accompanying drawings, the present invention will be further described in conjunction with specific embodiments, so as to better understand the present invention.
[0037] 1 Synthesis of host molecule Alg-β-CD
[0038] 1.1 Specific synthetic steps
[0039] Weigh 2.00 g of Alg into a round bottom flask, add 80 mL of distilled water, and dissolve it under mechanical stirring at room temperature for 6 h to obtain a homogeneous solution of sodium alginate (Alg) with a mass fraction of 2.5%, and adjust the solution with 0.5 mol / L HCl pH = 3.6, diluted with water to a mass fraction of 2%. Mono(6-amino-6-deoxy)-β-CD (1.37g, 1.3mmol), formaldehyde (1.8mmol) and cyclohexyl isonitrile (1.8mmol) were successively added to the above sodium alginate solution, mechanically Stir and react at room temperature for 24h. After the reaction, the reaction solution was diluted with water to 0.7 wt%, and dialyzed for 3 days using a dialysis bag with a molecular weight cut ...
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