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A device and method for testing the adhesion between gas hydrate and mineral particles

A technology of gas hydrate and mineral particles, which is applied in the direction of measuring devices, mechanical devices, earthwork drilling and mining, etc., to achieve significant practical value and accurate testing results

Active Publication Date: 2020-06-26
CHINA UNIV OF GEOSCIENCES (WUHAN)
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Generally, AFM can only be tested at normal pressure, and its detection laser will heat the probe, and when the temperature is higher than the gas hydrate phase equilibrium temperature, it will produce a phase change, so how to maintain the gas hydrate sample during the test Stability is the key issue whether this technology can be applied in the field of gas hydrate testing

Method used

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  • A device and method for testing the adhesion between gas hydrate and mineral particles
  • A device and method for testing the adhesion between gas hydrate and mineral particles
  • A device and method for testing the adhesion between gas hydrate and mineral particles

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Embodiment 1

[0057] The present invention will be further described in detail below in conjunction with the test experiment of the adhesion between carbon dioxide hydrate and mineral particles in the examples of the present invention.

[0058] S1. Selection of AFM probes: Select AFM silicon probes 1 with aluminum coating on the back, rectangular cantilever, and no needle tip, such as figure 2 shown. In this embodiment, the particle size of the mineral particles is about 20 μm, and the elastic constant of the selected probe 1 is about 35 N / m. The cantilever of the silicon probe 1 with this elastic constant is about 115 um in length, 35 um in width, and 3 um in thickness.

[0059] S2. Mineral particles adhered to the probe: figure 2 The mineral particles 2 shown are evenly dispersed in clear water, and a small amount of the prepared turbid liquid is dropped on the surface of the mica sheet substrate 3. After the water evaporates, the mineral particles 2 are dispersed on the surface of the...

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Abstract

A testing device for testing adhesion force includes a thermal insulated glove box, an atomic force microscope, a cryogenic sample stage, a high pressure gas source and a circulating chiller. The atomic force microscope includes a probe for adhering mineral particles. The cryogenic sample stage is configured for preparing gas hydrate sample. The cryogenic sample stage is arranged below the probe. The atomic force microscope and the cryogenic sample stage are placed in the thermal insulated glove box. The high pressure gas source provides pressure required for synthesis of gas hydrates, the high pressure gas source comprises a high pressure chamber covered on the cryogenic sample stage and a high pressure gas cylinder connected with the high pressure chamber. The circulating chiller, an outlet of the circulating chiller is connected with the thermal insulated glove box to control humidity and temperature inside the thermal insulated glove box.

Description

technical field [0001] The invention relates to the field of testing the adhesion of microparticles, in particular to a testing device and method for the adhesion between gas hydrates and mineral particles. Background technique [0002] Gas hydrate is one of the most potential unconventional and clean alternative energy sources after shale gas, coalbed methane and tight gas. It is mainly a crystallized ice-like "cage compound" formed by small molecule hydrocarbon gases such as methane and water under high pressure and low temperature conditions. It is estimated that the gas hydrate reserves in the South my country Sea alone are about 85 trillion cubic meters. Its exploitation and utilization are of great significance to alleviate the pressure of my country's energy shortage and adjust the energy structure. In May 2017, my country has successfully launched a trial mining project of gas hydrates in the Shenhu area of ​​the South China Sea, but how to safely, efficiently, long...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N19/04
CPCG01N19/04G01Q30/10G01Q30/12G01Q60/28E21B49/08E21B49/0875G01Q10/045G01Q60/38
Inventor 宁伏龙彭力李维王东东欧文佳刘志超孙嘉鑫
Owner CHINA UNIV OF GEOSCIENCES (WUHAN)
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