Preparation method of glossy transparent ultra-low-temperature glaze powder material

An ultra-low temperature, bulk material technology, applied in the field of preparation of glossy and transparent ultra-low temperature glaze powder materials, can solve the problems of limited application scope, waste of energy quality, high production cost, and achieve low price, low mineral content, and low ignition loss. Effect

Inactive Publication Date: 2019-02-19
WUYI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Existing low-temperature glazes generally contain frit, refractory components such as alumina and silicon oxide, and some strong fluxes such as lead oxide. However, the production cost of frit glaze is high and requires secondary firing. In addition, although lead can greatly reduce the firing temperature of the glaze, its toxicity limits its use in daily-use ceramics. range of applications, and is likely to cause environmental pollution

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] The preparation method of a glossy transparent ultra-low temperature glaze powder material described in Example 1 comprises the following steps:

[0020] (1) Weigh 34.4gB with a precision electronic balance 2 o 3 , 25.14gSiO2 2 , 5gAl 2 o 3 , 3.81gCaO, 11.74gZnO, 2.16gK 2 O, 16.11gNa 2 O, 1.04gBaO, 0.6g MgO, 48g borax, 1.2gSrO, 2.1g ball soil, 1.31gLi2O, 0.51gNa 5 P 3 o 10 raw materials;

[0021](2) Use a ball mill to grind raw materials to a fineness of 300 mesh sieves to form glaze powder, and the working speed is 25 rad / min to obtain ultra-low temperature glaze powder materials.

[0022] SiO 2 It is the main component of glaze and the main glass network former. SiO in glaze 2 The higher the content, the higher the firing temperature. SiO in low temperature glaze 2 The ratio to solvent is approximately 2:1 (mole); for glazes fired at the highest temperatures, this ratio rises to 10:1 (mole). However, increasing SiO 2 The content of the glaze can improve...

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Abstract

The invention discloses a preparation method of a glossy transparent ultra-low-temperature glaze powder material. The method comprises the following steps of (1) using a precision electronic balance for weighing 0-34.4 g of B2O3, 25.14-50 g of SiO2, 5-9.94 g of Al2O3, 3.81-7.58 g of CaO, 11.74-23.35 g of ZnO, 2.16-4.3 g of K2O, 1.57-16.11 g of Na2O, 1.04-2.07 g of BaO, 0.6-1.19 g of MgO, 48 g of borax, 1-1.2 g of SrO, 2.1-3.5 g of ball clay, 1.31-2.55 g of Li2O and 0.51-2.11 g of Na5P3O10 which are adopted as raw materials; (2) grinding the raw materials into 300 mesh sieve fineness through aball mill to form glaze powder at a working speed of 25 rad/min and then obtaining the ultra-low-temperature glaze powder material. The preparation method of the glossy transparent ultra-low-temperature glaze powder material utilizes the novel low-temperature fast-burning raw materials as fluxing agents for introducing alkali metal oxides or alkaline earth metal oxides, and since the raw materialsare characterized by completing a physicochemical reaction at a lower temperature, by utilizing this characteristic of the raw materials, low-temperature ceramic glaze is prepared, so that the purpose of fast burning at the low temperature is achieved. Moreover, the raw materials have few harmful impurities, less ignition loss, high melting performance and low viscosity at the high temperature, and a flat and smooth glaze surface is easily formed.

Description

technical field [0001] The invention relates to the technical field of ultra-low temperature glaze material technology, in particular to a preparation method of a glossy and transparent ultra-low temperature glaze powder material. Background technique [0002] Glaze is an extremely thin layer of glass applied to the surface of a ceramic body. According to the performance requirements of the green body, it uses ceramic raw materials and some chemical raw materials in a certain proportion, and melts under the action of high temperature to cover the surface of the green body with a glossy or matte glass layer. The purpose of glazing is to improve the surface properties of the body and improve the mechanical properties of the product. In terms of decoration, it can improve whiteness, gloss, increase color, and form colorful patterns; in terms of thermodynamic properties, it can improve hardness and heat stability; in terms of chemical properties, it can increase acid and alkali...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C8/00
CPCC03C8/00
Inventor 尹荔松安科云涂驰周马思琪蓝键
Owner WUYI UNIV
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