Rubber composition and vulcanized rubber for vehicle tire sidewall, preparation method and application thereof
A rubber composition and vulcanized rubber technology are applied in the application of vulcanized rubber and vulcanized rubber in the tire sidewall, and the field of preparing vulcanized rubber, which can solve the problem of high strength and low rolling resistance of tire sidewall rubber, affecting the overall performance of composite materials, and high process control requirements. problem, to achieve the effect of good dynamic flexural flexibility, increased strength, and improved flexural resistance
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[0066]In order to specifically explain the method of preparing a vulcanized rubber of the present invention, there is provided a preferred embodiment of the preferred embodiment.
[0067](1) Place the rubber substrate in the mesh, the rotation speed is 50 to 120 rpm, the initial kicking temperature is 70 ~ 90 ° C, and the plastic flowing time is 0.1 to 1 min under conditions; then rubber modification The component A is introduced into the above-mentioned mesh for first kneading to obtain a phase of a master.
[0068](2) The one-stage master gel is added to the mesenchymal mixture for 3-5 hours in the mesh, which is added to the mesenter-containing mixture of white carbon black, carbon black, activator, anti-aging agent and softener. Get two-stage masterpiece;
[0069](3) Set the rotation speed of the unfaming machine to be 50 ~ 100 rpm, the initial kicking temperature is 25 ~ 50 ° C, after plasticizing the two - stage master gum, adding the component C containing the accelerator and sulfuriz...
Embodiment 1
[0101]Rubber composition formula: 60 parts by weight of natural rubber, 40 parts by weight of the tenth rubber, 3-mercaptopropionic acid (rubber modifier) 3 parts by weight, carbon black N550 20 parts by weight, carbon black N330 30 parts by weight, TDAE (softener), 4 parts by weight, stearic acid (activator), 0.5 parts by weight of sulfur (vulcanizing agent), 5 weight, TBBS (accelerator) Part, anti-aging agent 4020 (anti-aging agent) 1 part by weight.
[0102]Preparation process of vulcanized rubber:
[0103](1) The rubber substrate, rubber modifier is first mixed, resulting in a mapping; specifically, the natural rubber, a tall-dicyser is added to the intimer, and the rotational speed is 80 rpm, and the initial kneading temperature is 80 ° C. The raw gum is 0.5 min; the rubber modifier is added to the above-mentioned mesh, the mixing temperature is 90 ° C, the kneading time is 7 minutes, resulting in a phase of the master glue;
[0104](2) The second blend of the one-stage master gel and...
Embodiment 2
[0109]Rubber composition formula: 40 parts by weight of natural rubber, 60 parts by weight of TDB, 4-mercaptobutyric acid (rubber modifier) 8 parts by weight, white carbon black 50 parts by weight, carbon black N550 parts by weight, TDAE (softening 5 parts by weight, zinc oxide (activator) 4 parts by weight, stearic acid (activator) 3 parts by weight, sulfur (vulcanizing agent) 4 parts by weight, accelerator D (promoter) 1000 parts, anti-aging agent 4020 (Anti-aging) 2 parts by weight.
[0110]Preparation process of vulcanized rubber:
[0111](1) The rubber substrate, rubber modifier is first mixed, resulting in a mapping; specifically, the natural rubber, a tall-dicyser is added to the intimer, and the rotational speed is 80 rpm, and the initial kneading temperature is 80 ° C. The raw gum is 0.5 min; the rubber modifier is added to the above-mentioned mesh, the mixing temperature is 100 ° C, the kneading time is 5 min, resulting in a phase of the master glue;
[0112](2) The second blend ...
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