High-temperature-resistant and high-pressure-resistant rubber material as well as preparation method and application thereof

A technology of rubber material and high pressure resistance, applied in the fields of high pressure resistance rubber material and high temperature resistance, can solve the problems of increasing the technical difficulty and cost of domestic deep well and ultra-deep well mining, undisclosed technical measures, and high cost of packers, etc. The effect of improving H2S resistance, improving operation performance and improving service life

Inactive Publication Date: 2019-03-01
CHINA PETROCHEMICAL CORP +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, based on foreign technical blockade, they only provide domestic finished materials or parts at high prices, and do not disclose the corresponding technical measures, let alone provide correspon

Method used

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  • High-temperature-resistant and high-pressure-resistant rubber material as well as preparation method and application thereof
  • High-temperature-resistant and high-pressure-resistant rubber material as well as preparation method and application thereof
  • High-temperature-resistant and high-pressure-resistant rubber material as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0025] Example 1

[0026] The present invention is composed of the following raw materials in mass percentages: 62% tetrapropylene fluorine rubber, 22.9% carbon black, 0.8% stearic acid, 7% graphene, 0.8% magnesium oxide, 1.5% dicumyl peroxide, triene Propyl isocyanurate 4%, triethoxysilane 1%.

[0027] In the above formula, the tetrapropylene fluorine rubber is tetrapropylene fluorine raw rubber, the dynamic shear storage modulus of the tetrapropylene fluorine raw rubber is 340KPa, and the Mooney viscosity value is 160 at a temperature of 100°C.

[0028] In the above formula, the graphene is graphene oxide, and the sheet diameter of the graphene is 3 μm.

[0029] In the above formula, triethoxysilane is a mixture of methyltriethoxysilane and vinyltriethoxysilane, and the mixing ratio is 1:1.

[0030] The preparation method of the present invention is:

[0031] The components in the formula raw materials are in accordance with tetrapropylene fluorine rubber, carbon black, stearic acid, ...

Example Embodiment

[0035] Example 2

[0036] The present invention is composed of the following raw materials in mass percentage: tetrapropylene fluorine rubber 67.8%, carbon black 18%, stearic acid 0.7%, graphene 6%, magnesium oxide 0.5%, dicumyl peroxide 2%, triene Propyl isocyanurate 3%, triethoxysilane 2%.

[0037] In the above formula, the tetrapropylene fluorine rubber is tetrapropylene fluorine raw rubber, the dynamic shear storage modulus of the tetrapropylene fluorine raw rubber is 340KPa, and the Mooney viscosity value is 160 at a temperature of 100°C.

[0038] In the above formula, the graphene is graphene oxide, and the sheet diameter of the graphene is 4 μm.

[0039] In the above formula, triethoxysilane is a mixture of methyltriethoxysilane and vinyltriethoxysilane, and the mixing ratio is 1:1.

[0040] The preparation method of the present invention is:

[0041] The components in the formula raw materials are in accordance with tetrapropylene fluorine rubber, carbon black, stearic acid, gra...

Example Embodiment

[0045] Example 3

[0046] The present invention is composed of the following raw materials in mass percentages: tetrapropylene fluorine rubber 65%, carbon black 19.5%, stearic acid 0.7%, graphene 7.5%, magnesium oxide 0.7%, dicumyl peroxide 1.7%, triene Propyl isocyanurate 3.4%, triethoxysilane 1.5%.

[0047] In the above formula, the tetrapropylene fluorine rubber is tetrapropylene fluorine raw rubber, the dynamic shear storage modulus of the tetrapropylene fluorine raw rubber is 340KPa, and the Mooney viscosity value is 160 at a temperature of 100°C.

[0048] In the above formula, the graphene is graphene oxide, and the sheet diameter of the graphene is 5 μm.

[0049] In the above formula, triethoxysilane is a mixture of methyltriethoxysilane and vinyltriethoxysilane, and the mixing ratio is 1:1.

[0050] The preparation method of the present invention is:

[0051] The components in the formula raw materials are in accordance with tetrapropylene fluorine rubber, carbon black, stearic ...

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Abstract

The invention discloses a high-temperature-resistant and high-pressure-resistant rubber material as well as a preparation method and application thereof. The rubber material is prepared from the following raw materials in percentage by mass: 60-70% of tetrafluoroethylenepr-opylene copolymer, 15-25% of carbon black, 0.5-1% of stearic acid, 5-10% of graphene, 0.5-1% of magnesium oxide, 1.5-2% of dicumyl peroxide, 3-4% of triallyl isocyanurate and 1-2% of triethoxysilane. According to the high-temperature-resistant and high-pressure-resistant rubber material as well as the preparation method andthe application thereof, the components are synergistic and compatible, the prepared rubber material can bear a high temperature of 205 DEG C and a high pressure difference of 105 MPa at the same time, the high-temperature-resistant performance and the high-pressure-resistant performance are excellent, the resistance to a high hydrogen sulfide environment with 20% H2S is achieved, the economic benefits are remarkable, and the application prospect is good.

Description

technical field [0001] The invention relates to a rubber material, in particular to a high-temperature-resistant and high-pressure-resistant rubber material, as well as a preparation method and application of the rubber material. Background technique [0002] As a polymer compound material with the characteristics of elasticity, insulation, impermeability, and airtightness, rubber materials have been widely used in industry and life, including the application of downhole tool packers for oil and gas production. [0003] In oil and gas production, the packer is used to isolate the annular space between the central pipe string and the wellbore, and between the pipe string, so as to isolate the production layer and realize the control of production (injection) fluid. The setting of the packer in the downhole is mainly realized through the rubber sleeve formed by rubber material, and the stability and reliability of the rubber sleeve under the downhole working conditions directl...

Claims

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Application Information

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IPC IPC(8): C08L27/12C08K13/02C08K3/04C08K5/09C08K3/22C08K5/14
CPCC08K3/04C08K3/042C08K3/22C08K5/09C08K5/14C08K13/02C08K2003/222C08K2201/003C08L2201/08C08L2312/00C08L27/12
Inventor 铁忠银任俊松李晖吕占春郭明扬陈华龙
Owner CHINA PETROCHEMICAL CORP
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