Unlock instant, AI-driven research and patent intelligence for your innovation.

A Precise and Continuous Controlling Method of Water Adhesion on PTFE Surface

A polytetrafluoroethylene and adhesion technology, used in metal processing equipment, welding equipment, manufacturing tools, etc., can solve the problems of cumbersome preparation procedures, large environmental pollution, slow processing speed, etc., to achieve simple and effective operation methods, environmental protection low pollution effect

Active Publication Date: 2020-07-10
HUAZHONG UNIV OF SCI & TECH
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Aiming at the above defects or improvement needs of the prior art, the present invention provides a precise and continuous control method for the surface water adhesion of polytetrafluoroethylene, which uses a picosecond laser to treat the surface of polytetrafluoroethylene, and controls the appropriate Laser processing parameters, using the unique energy characteristics of the picosecond laser and the specific material of PTFE, the picosecond laser produces a certain range of heat-affected areas on the surface of PTFE, with the help of the picosecond laser and the surface of PTFE Interaction, to achieve accurate and continuous controllable water adhesion on the surface of PTFE, correspondingly not only can obtain a PTFE surface with a specific water adhesion value; but also can obtain a series of water with precise continuous Several polytetrafluoroethylene surfaces with different adhesion strengths can meet different application requirements, thereby solving the cumbersome preparation procedures, slow processing speed, low efficiency, Environmental pollution is high, cost is high, and the focus is on technical issues such as difficulty in achieving continuous and precise control

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A Precise and Continuous Controlling Method of Water Adhesion on PTFE Surface
  • A Precise and Continuous Controlling Method of Water Adhesion on PTFE Surface
  • A Precise and Continuous Controlling Method of Water Adhesion on PTFE Surface

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0053] (1) Set the picosecond laser processing parameters, use a picosecond laser with a wavelength of 355nm, the laser spot diameter is 10μm, the scanning speed is 1000mm / s, the pulse frequency is 200KHz, the output power is 5W, and the laser scanning distance is changed from 5μm to 140μm, the increased width of each laser scan, that is, the scan step length is 5μm, on the focal plane, the surface clean PTFE is processed.

[0054] Then, the structure and properties of the laser-processed surface were determined.

[0055] figure 1 A scanning electron microscope (SEM) image of a non-laser-processed PTFE surface. It can be seen that the surface of PTFE without laser processing is very smooth and flat.

[0056] figure 2 It is the scanning electron microscope (SEM) picture when the laser scanning distance is 80 μm and 130 μm, respectively. It can be seen from the figure that when the laser scanning distance is 80 μm, the laser etching forms a square columnar protrusion, and t...

Embodiment 2

[0061] Put the polytetrafluoroethylene in acetone, absolute ethanol and distilled water, respectively, and use ultrasonic waves to clean each for 5 minutes to remove the pollutants adhered to the surface, and then dry to obtain a clean polytetrafluoroethylene surface.

[0062] Use a picosecond laser with a wavelength of 355nm, the laser spot diameter is 10μm, set the laser scanning rate to 1500mm / s, the pulse frequency to 200KHz, the output power to 8W, set the scanning step to 10μm, and set the laser scanning spacing to 60μm, 70μm, 80μm, 90μm, 100μm, 110μm and 120μm.

[0063] An optical contact angle measuring instrument was used to measure the rolling angle of water droplets on the surface of polytetrafluoroethylene after laser etching, and the test results are shown in Table 1 below.

[0064] Table 1: Example 2 shows the rolling angle of the surface of the polytetrafluoroethylene material prepared under different laser scanning distances.

[0065]

[0066]

[0067] I...

Embodiment 3

[0069] Put the polytetrafluoroethylene in acetone, absolute ethanol and distilled water, respectively, and use ultrasonic waves to clean each for 5 minutes to remove the pollutants adhered to the surface, and then dry to obtain a clean polytetrafluoroethylene surface.

[0070] Use a picosecond laser with a wavelength of 355nm, the laser spot diameter is 10μm, set the laser scanning rate to 1300mm / s, the pulse frequency to 200KHz, the output power to 6.5W, set the scanning step to 5μm, and set the laser scanning spacing respectively 55μm, 60μm, 65μm, 70μm, 75μm, 80μm, 85μm, 90μm, 95μm, 100μm, 105μm, 115μm and 120μm.

[0071] An optical contact angle measuring instrument was used to measure the rolling angle of water droplets on the surface of polytetrafluoroethylene after laser etching, and the test results are shown in Table 2 below.

[0072] Table 2: Example 3 shows the rolling angle of the surface of the polytetrafluoroethylene material prepared under different laser scannin...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
diameteraaaaaaaaaa
wavelengthaaaaaaaaaa
Login to View More

Abstract

The invention belongs to the field of laser surface treatment and micro-processing, and particularly relates to an accurate and continuous regulation and control method for the water adhesion force ofthe surface of polytetrafluoroethylene. According to the method, surface treatment is carried out on the polytetrafluoroethylene by using picosecond laser; by means of controlling appropriate laser processing parameters and utilizing specific energy characteristics of the picosecond laser and specific materials of the polytetrafluoroethylene, a certain range of heat-affected zone is generated onthe surface of the polytetrafluoroethylene by the picosecond laser; and by means of the interaction between the picosecond laser and the surface of the polytetrafluoroethylene, the water adhesion force of the surface of the polytetrafluoroethylene can be accurately and continuously controlled, and therefore the technical problems that the producing method of an existing water adhesion force controllable super-hydrophobic surface is tedious in procedure, low in processing speed and efficiency, large in environmental pollution, high in cost, incapable of realizing continuous and accurate controleasily and the like are solved.

Description

technical field [0001] The invention belongs to the field of laser surface treatment and micromachining, and more specifically relates to a method for precise and continuous control of water adhesion on the surface of polytetrafluoroethylene. Background technique [0002] The superhydrophobic surface refers to the surface with a water static contact angle greater than 150°. According to the different surface water adhesion, there are two typical structures in the superhydrophobic surface: one is a structure similar to the surface of a lotus leaf, and the structure With ultra-low water adhesion, it is difficult for water droplets to stay on its surface, showing good self-cleaning ability; the other is a structure similar to the surface of rose petals, which has ultra-high water adhesion, regardless of No matter how inclined the surface is, water droplets can firmly adhere to the surface. [0003] The controllable water adhesion refers to adjusting the preparation process and...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): B23K26/00B23K26/362B23K26/352
CPCB23K26/00B23K26/352B23K26/362
Inventor 刘建国秦中立艾骏曾晓雁
Owner HUAZHONG UNIV OF SCI & TECH