Acrylate emulsion for building interior wall paint and preparation method thereof, and paint
A technology of acrylate and butyl acrylate, which is applied in the field of acrylate emulsion for architectural interior wall coatings and its preparation, can solve the problems of increasing formula cost, etc., achieve excellent scrub resistance and freeze-thaw stability, low VOC content, and environmental protection sex effect
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[0040] The embodiment of the present invention proposes a kind of preparation method of above-mentioned acrylic ester emulsion for architectural interior wall coating, comprises the following steps:
[0041] a) Pre-emulsification I: At normal temperature and pressure, mix 0.1-0.4 parts of reactive anionic emulsifier, 0.1-0.4 parts of reactive nonionic emulsifier and 20-30 parts of water in an emulsification tank, stir, and then add 5 parts in sequence -15 parts of butyl acrylate, 15-23 parts of styrene, 5-15 parts of isooctyl acrylate, 0.1-0.5 parts of self-crosslinking monomer, 0.1-2 parts of carboxyl monomer, 0.1-1 part of acrylamide, 0.01- 0.1 part of silane coupling agent, stirred to obtain pre-emulsion I;
[0042] b) Polymerization I: Add 0.1-0.4 parts of reactive anionic emulsifier, 0.1-0.4 parts of reactive nonionic emulsifier and 4.5-15 parts of water into the reactor, heat up to 80-87 °C, add 0.01-0.1 parts of After the sulfate reaction, start dripping persulfate sol...
Embodiment 1
[0058] An acrylic ester emulsion for building interior wall paint is prepared by comprising the following raw materials in parts by weight:
[0059]
[0060]
[0061] The preparation method of above-mentioned acrylic acid ester emulsion for building interior wall paint, comprises the following steps:
[0062] a) Pre-emulsification I: At normal temperature and pressure, mix 0.3 parts of reactive anionic emulsifier, 0.17 parts of reactive nonionic emulsifier and 23.4 parts of water in an emulsification tank, stir well and dissolve evenly, and then add 10 parts of butyl acrylate in sequence Esters, 21.4 parts of styrene, 9.5 parts of isooctyl acrylate, 0.22 parts of self-crosslinking monomers, 1.25 parts of carboxyl monomers, 0.59 parts of acrylamide, 0.04 parts of silane coupling agent, fully stirred and dissolved evenly, that is, pre-emulsified Liquid I;
[0063] b) Polymerization I: Add 0.34 parts of reactive anionic emulsifier, 0.3 parts of reactive nonionic emulsifier...
Embodiment 2
[0070] An acrylic ester emulsion for building interior wall paint is prepared by comprising the following raw materials in parts by weight:
[0071]
[0072] The preparation method of the acrylic ester emulsion for the above-mentioned architectural interior wall paint is the same as in Example 1.
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