Polishing boron sulfate rust remover
A technology of sulfate ester and rust removal liquid, applied in the field of rust removal, can solve the problems of increasing processing cost, affecting steel strength, hydrogen embrittlement, etc., achieving the effect of short rust removal time and preventing oxidation
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Embodiment 1
[0024] 1. First prepare the boron sulfate ester rust removal solution, the preparation steps are as follows:
[0025] (1) Put 55 parts of nonylphenol into the reaction kettle, heat to 105°C, then slowly add 2 parts of boric acid, and react for 135 minutes after the addition;
[0026] (2) After the reaction is completed, the temperature is lowered to 66°C, 3 parts of auxiliary glycerol are added, and the temperature is naturally lowered to room temperature;
[0027] (3) Slowly add 1.5 parts of S under vacuum 2 O 3 , Stir while adding, heat up to 55°C after adding, and react for 150 minutes;
[0028] (4) After the reaction is completed, the temperature is lowered to below 50°C, and 2.5 parts of auxiliary glycerin is added, reacted for 110 minutes, and then the temperature is naturally lowered to below 30°C to obtain.
[0029] 2. Mix the prepared borosulfate rust removal liquid with alumina particles with a particle size of 0.3 microns and water, and stir them evenly; the mass of alumina p...
Embodiment 2
[0032] 1. First prepare the boron sulfate ester rust removal solution, the preparation steps are as follows:
[0033] (1) Put 70 parts of nonylphenol polyoxyethylene ether NP-10 into the reactor, heat to 130°C, then slowly add 6 parts of boric acid, and react for 120 minutes after the addition;
[0034] (2) After the reaction is completed, the temperature is lowered to 75°C, 5 parts of sorbitol are added as an auxiliary agent, and the temperature is naturally lowered to room temperature;
[0035] (3) Slowly add 3 parts of SO under vacuum 3 , Stir while adding, heat up to 80°C after adding, react for 125 minutes;
[0036] (4) After the reaction is completed, the temperature is lowered to below 50°C, and 5 parts of epoxy soybean oil is added as an auxiliary agent, reacted for 130 minutes, and then the temperature is naturally lowered to below 30°C to obtain.
[0037] 2. Mix the prepared borosulfate rust removing liquid with alumina particles with a particle size of 1 micron and water, and...
Embodiment 3
[0040] 1. First prepare the boron sulfate ester rust removal solution, the preparation steps are as follows:
[0041] (1) Put 95 parts of nonylphenol polyoxyethylene ether NP-20 into the reactor, heat to 145°C, then slowly add 13 parts of boric acid, and react for 110 minutes after the addition;
[0042] (2) After the reaction is completed, the temperature is lowered to 95°C, 11 parts of the auxiliary propylene glycol are added, and the temperature is naturally lowered to room temperature;
[0043] (3) Slowly add 4.5 parts of S under vacuum 2 O 3 , Stir while adding, heat up to 95°C after adding, and react for 150 minutes;
[0044] (4) After the reaction is completed, the temperature is lowered to below 50°C, 9 parts of mannitol are added as an auxiliary agent, reacted for 180 minutes, and then the temperature is naturally lowered to below 30°C to obtain.
[0045] 2. Mix the prepared boron sulfate ester rust removal solution with zinc oxide particles with a particle size of 3 microns an...
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