Carbon nitride based material for photocatalytic water total decomposition as well as preparation and application thereof
A carbon nitride-based, photocatalytic technology, used in chemical instruments and methods, physical/chemical process catalysts, electrolysis processes, etc., can solve problems such as deactivation, and achieve the effects of inhibiting separation, preventing rapid recombination, and high stability
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[0035] A carbon nitride-based material for photocatalytic total water decomposing includes a carbon nitride carrier, the carbon nitride carrier is loaded with monoatomic palladium, and the loading of monoatomic palladium is 0.0925wt.%.
[0036] The carbon nitride-based material for photocatalytic total water dissolution is prepared by the impregnation-high temperature anchoring method, that is, monoatomic palladium is loaded on the surface and between the carbon nitride layers. The quality of the palladium in the palladium source in this embodiment is comparable to that of graphite. The mass ratio of phase carbon nitride is 0.0016:1. The specific steps are:
[0037] Weigh 10g of melamine and place it in a crucible, then put the crucible in a muffle furnace, raise it to 500℃ at a heating rate of 2℃ / min, then heat it for 2 hours, then raise it to 520℃ at the same temperature After 2 hours, after naturally cooling to room temperature, the obtained massive solid was gr...
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