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Rare earth halide scintillating material and application thereof

A technology of scintillation materials and halides, which is applied in the direction of rare earth metal halides, rare earth metal chlorides, luminescent materials, etc., can solve the problems of poor consistency of crystal scintillation performance and complex components, so as to avoid uneven segregation, The effect of excellent energy resolution and energy response linearity

Active Publication Date: 2019-07-09
GRIREM ADVANCED MATERIALS CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this scheme also has its disadvantages, that is, the components are relatively complex, and the consistency of crystal scintillation performance will be poor due to the uneven distribution of different ions.

Method used

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  • Rare earth halide scintillating material and application thereof

Examples

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Comparison scheme
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Embodiment 1

[0041] Accurately weigh 119.89g of anhydrous LaBr in an Ar atmosphere protected glove box 3 (purity is 99.99%), 6.33g anhydrous CeBr 3 (purity is 99.99%) and 1.852g metal La (purity is 99.99%), mix uniformly and put into a quartz crucible with a diameter of 25mm. The rest of the operations are the same as in Comparative Example 1.

[0042] Embodiment 2-13 is all the same as embodiment 1 except that the ratio of raw materials is different.

[0043] The detailed comparative situation of all embodiments and comparative examples is shown in Table 1.

[0044] Table 1:

[0045]

[0046] It can be seen from the above description that, compared with undoped or alkaline earth metal doped, alkaline earth metal and halogen ion co-doped crystals with the same composition, the non-integer ratio crystals of the present invention have extremely excellent scintillation properties, reflecting the Obvious performance advantage. While ensuring the high performance of the material, the co...

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Abstract

The invention provides a rare earth halide scintillating material and application thereof. The general chemical formula of the rare earth halide scintillating material is REaCebX3, wherein RE is a rare earth element La, Gd, Lu or Y, X is one or two of halogens Cl, Br and I, a is more than or equal to 0 and less than or equal to 1.0, b is more than or equal to 0.01 and less than or equal to 1.1, and the sum of a and b is more than or equal to 1.0001 and less than or equal to 1.2. A rare earth halide having a +2 valence and with the same component is used as a doping agent to replace a heterogeneous alkaline earth metal halide in the prior art for doping, and therefore, the rare earth halide scintillating material is relatively short of halogen ions, the apparent valence of the rare earth ions is between +2 and +3, the rare earth halide scintillating material belongs to a non-stoichiometric compound, but the crystal structure of the original stoichiometric compound is still maintained, and the rare earth halide scintillating material has more excellent energy resolution and energy response linearity than the stoichiometric compound.

Description

technical field [0001] The invention relates to the field of inorganic scintillation materials, in particular to a rare earth halide scintillation material and its application. Background technique [0002] Scintillation materials can be used to detect high-energy rays such as α-rays, γ-rays, and X-rays, and high-energy particles such as neutrons, and are widely used in nuclear medicine, high-energy physics, safety inspection, oil logging and other fields. [0003] Scintillation materials are usually applied in the form of single crystals, and in some cases can also be ceramics or other forms. Different application fields have different performance requirements for scintillation materials. However, for most applications, scintillation materials are expected to have as high a light yield as possible, as short a decay time as possible, and as high an energy resolution as possible. Especially for nuclear medicine imaging devices such as positron emission tomography (PET) scan...

Claims

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Application Information

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IPC IPC(8): C09K11/85C30B29/12G01T1/202E21B47/00
CPCC09K11/7719C09K11/7772C30B29/12G01T1/2023E21B47/00C09K11/08C09K11/77C01F17/253C01F17/271C01P2002/54C30B11/00E21B49/00G01T1/2985G01T1/362
Inventor 余金秋刁成鹏张辉吴浩崔磊何华强
Owner GRIREM ADVANCED MATERIALS CO LTD
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