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Methanol synthesizing device and method of using methanol synthesizing device for synthesizing methanol

A methanol synthesis and methanol technology, which is applied in chemical instruments and methods, preparation of organic compounds, preparation of hydroxyl compounds, etc., can solve the problems of small loading of single-column synthesis catalysts, high effective carbon in purge gas, and low conversion rate per pass. , to achieve the effect of improving the overall operating efficiency, improving the C conversion rate, and reducing the pressure of the synthesis system

Pending Publication Date: 2019-07-30
HEBEI JINNIU RISUN CHEM CO LTD
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Problems solved by technology

[0007] This single-tower cycle synthesis system mainly has two disadvantages. One is that the single-tower synthesis catalyst has a small loading capacity, a high space velocity, and a low single-pass conversion rate. Therefore, in order to maintain a high single-pass conversion rate, it is necessary to operate at the upper limit of the operating pressure. , not only increased power consumption, but also a great potential safety hazard; the second is that the effective carbon in the exhaust gas is high, and the average content of CO in the exhaust gas is 3% (v), CO 2 The average content of 4% (v)

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  • Methanol synthesizing device and method of using methanol synthesizing device for synthesizing methanol

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Embodiment 1

[0066] like figure 1 The setup for methanol synthesis is shown. Based on the original single-tower synthesis system, the device is connected in parallel with a second synthesis tower (43) to reduce the space velocity and increase the single-pass conversion rate of total carbon. Simultaneously, the outlet of the original exhaust gas is connected in series with the third synthesis tower (81).

[0067] In this methanol synthesis unit (200,000 tons / year), the catalyst content of the first synthesis tower (41) is 40 cubic meters, and the synthesis gas space velocity is 10000h -1 , the reaction pressure is 6.9Mpa, the reaction temperature is 200-250°C, the catalyst content of the second synthesis tower is 20 cubic meters, and the synthesis gas space velocity is 10000h -1 , reaction, synthesis gas space velocity is 6500h -1 , the reaction pressure is 5.5-6.0Mpa, the reaction temperature is 200-250°C, the catalyst content of the third synthesis tower is 4-6 cubic meters, and the sy...

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Abstract

The invention relates to a methanol synthesizing device and a method of using the methanol synthesizing device for synthesizing methanol. According to the methanol synthesizing device, it is unnecessary to replace original equipment on a large scale, and after pipeline connection is slightly adjusted, the original methanol synthesizing device can be used for production, so that the methanol synthesizing device is popularized among a large number of methanol companies. The method is easy to implement, only electricity consumption of a small synthesis circulating machine and little cooling waterconsumption are improved, and production requirements can be met simply by adopting original public and auxiliary facilities and few additionally arranged pipelines. After the methanol synthesizing device is transformed and put into operation, the overall running efficiency of the methanol synthesizing device is significantly improved; the pressure of a synthesis system is at a low level, not only is power consumption reduced, but also the safety of the device is significantly improved, the total carbon (C) conversion rate is also increased, and energy saving and emission reduction are achieved.

Description

technical field [0001] The invention relates to a methanol synthesis device and a method for synthesizing methanol using the device. Specifically, the invention relates to a methanol synthesis device with a specific multi-tower structure and a method for synthesizing methanol using the device. Background technique [0002] Methanol is a commonly used chemical raw material, which has a wide range of applications in many fields. For example, it can be used as a solvent, antifreeze, fuel or denaturant, and can also be used to produce biodiesel through transesterification, etc. [0003] In the prior art, the conventional preparation method of methanol is, under the action of catalyst, by methanol synthesis gas (the main component is H 2 , CO and CO 2 ) reaction generates methyl alcohol, and its reaction formula is as follows: [0004] CO+2H 2 →CH 3 OH+90.73kJ / mol [0005] CO 2 +3H 2 →CH 3 OH+H 2 O+48.02kJ / mol [0006] For the reaction process, the traditional coke ove...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C29/152C07C31/04
CPCC07C29/152C07C31/04
Inventor 张恰王灵清李庆华郎莹赵德旭石志哲孔力军王海平张燕
Owner HEBEI JINNIU RISUN CHEM CO LTD
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