Preparation method of gendarussa vulgaris essential oil
A technology of bone refusal and essential oil, which is applied in the field of traditional Chinese medicine, can solve the problems of troublesome application, inability to achieve a good therapeutic effect, and difficulty in carrying, etc., and achieve the effect of improving the therapeutic effect, being easy to use and carry, and reducing pain.
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Embodiment 1
[0024] A preparation method of Xiaobagu essential oil, comprising the following steps:
[0025] (1) Select clean and fresh small ribs for cleaning, and the cleaning time is 6 minutes;
[0026] (2) Water control is carried out to the small bone barge after cleaning, and the small bone barge after water control is evenly cut into sections by a cutting machine, and the length of the cut section is 3cm;
[0027] (3) Carry out heat pump low-temperature drying to the small ribs after cutting with a heat pump low-temperature dryer, and the drying time is 6 hours;
[0028] (4) Control the working temperature of the pulverizer at 18° C., and carry out low-temperature pulverization to the dried small ribs until they are pulverized to 50 mesh;
[0029] (5) Perform supercritical CO on the pulverized small bones 2 Extract to obtain extract A, the temperature is 50°C, the pressure is 30Mpa, the flow rate is 18L, and the time is 50min;
[0030] (6) Carry out molecular distillation purific...
Embodiment 2
[0036] A preparation method of Xiaobagu essential oil, comprising the following steps:
[0037] (1) Select clean and fresh small ribs for cleaning, and the cleaning time is 8 minutes;
[0038] (2) Water control is carried out to the small rib after cleaning, and the small rib after water control is evenly cut into sections by a cutting machine, and the length of the cut is 5cm;
[0039] (3) Carry out heat pump low-temperature drying to the small ribs after sectioning with a heat pump low-temperature dryer, and the drying time is 8 hours;
[0040] (4) Control the working temperature of the pulverizer at 25° C., and carry out low-temperature pulverization to the dried small ribs until they are pulverized to 60 mesh;
[0041] (5) Perform supercritical CO on the pulverized small bones 2 Extract to obtain extract A, the temperature is 50°C, the pressure is 28Mpa, the flow rate is 20L, and the time is 55min;
[0042] (6) Carry out molecular distillation purification to A to obtai...
Embodiment 3
[0048] A preparation method of Xiaobagu essential oil, comprising the following steps:
[0049] (1) Select clean and fresh small ribs for cleaning, and the cleaning time is 10 minutes;
[0050] (2) Water control is carried out to the small rib after cleaning, and the small rib after water control is evenly cut into sections by a cutting machine, and the length of the cut is 5cm;
[0051] (3) Carry out heat pump low-temperature drying to the small ribs after cutting with a heat pump low-temperature dryer, and the drying time is 6 hours;
[0052] (4) Control the working temperature of the pulverizer at 30° C., and carry out low-temperature pulverization to the dried small ribs until they are pulverized to 55 mesh;
[0053] (5) Perform supercritical CO on the pulverized small bones 2 Extract to obtain extract A, the temperature is 50°C, the pressure is 32Mpa, the flow rate is 20L, and the time is 55min;
[0054] (6) carry out molecular distillation purification to A to obtain ...
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