Preparation method of zinc sulfide cadmium solid solutions with different morphologies
A zinc cadmium sulfide, solid solution technology, applied in the field of photocatalytic materials, can solve the problems of low photocatalytic hydrogen production performance, high preparation cost, complex preparation process, etc., achieve high photocatalytic hydrogen production performance, easy control of the process, and preparation method. simple effect
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[0026] The present invention will be described in further detail below in conjunction with the accompanying drawings and specific embodiments.
[0027] A preparation method of zinc cadmium sulfide solid solution with different shapes, which specifically comprises the following steps:
[0028] Step 1. Take L-cysteine and Zn(Ac) according to the molar ratio of 4-5:1:1 2 2H 2 O, Cd(Ac) 2 2H 2 O is dissolved in ethylene glycol or a mixed solution of ethylene glycol and deionized water, and vigorously stirred at a speed of 800 to 1000 rpm for 25 to 35 minutes to form a suspension; the volume ratio of ethylene glycol to deionized water is 1 / 9~10 / 0;
[0029] Step 2. Transfer the suspension to a polytetrafluoroethylene reactor, heat to 160°C-230°C for 23-25 hours, cool to room temperature after the reaction, centrifuge to obtain a precipitate, and use deionized water and absolute ethanol to separate After repeated washing of the precipitate, it was vacuum-dried at 55-65° C. ...
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