A kind of organosilicon leveling agent that can improve coating recoating performance and its application
A technology of silicone leveling agent and coating, applied in the field of silicone leveling agent, can solve the problems of poor overcoating performance and poor adhesion of coatings
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Embodiment 1
[0041] Example 1 A silicone leveling agent is provided, its preparation raw materials include hydrogen-containing silicone oil and functional monomer; the silicone leveling agent is prepared by the following method: 20g of hydrogen-containing silicone oil, 9.8g of functional monomer and 0.005g of platinum Add the rhodium complex into the reactor, add 120ml of acetone and ethyl acetate mixed solvent (volume ratio 3:2) and stir to dissolve, and react at 60°C for 4 hours, cool down to room temperature, concentrate and dry.
[0042] The hydrogen-containing silicone oil is IOTA203 low hydrogen-containing silicone oil (hydrogen content 0.36wt%) from Anhui Aiyota Silicone Oil Co., Ltd.; the functional monomer is trifluoroethyl methacrylate (CAS: 352-87-4) .
[0043] This example also provides a coating with good recoating performance using the above-mentioned organic silicon leveling agent. 3.
[0044] Described acrylic resin is the RP002 type acrylic resin of BASF; Described epox...
Embodiment 2
[0045] Example 2 Provide a kind of silicone leveling agent, its preparation raw material comprises hydrogen-containing silicone oil and functional monomer; Described silicone leveling agent is prepared by the following method: 20g hydrogen-containing silicone oil, 6.5g functional monomer and 0.002g platinum Add the rhodium complex into the reaction kettle, add 120ml of acetone and ethyl acetate mixed solvent (volume ratio 3:2) and stir to dissolve, and react at 60°C for 3 hours, cool down to room temperature, concentrate and dry.
[0046] The hydrogen-containing silicone oil is IOTA203 low hydrogen-containing silicone oil (0.75 wt% hydrogen content) from Anhui Aiyota Silicone Oil Co., Ltd.; the functional monomer is trifluoroethyl methacrylate (CAS: 352-87-4) .
[0047] This example also provides a coating with good recoating performance using the above-mentioned organic silicon leveling agent. 8.
[0048] Described acrylic resin is the RP002 type acrylic resin of BASF; De...
Embodiment 3
[0049] Example 3 Provide a kind of silicone leveling agent, its preparation raw material comprises hydrogen-containing silicone oil and functional monomer; Described silicone leveling agent is prepared by following method: 20g hydrogen-containing silicone oil, 8g functional monomer and 0.004g platinum-rhodium Add the complex to the reaction kettle, add 120ml of acetone and ethyl acetate mixed solvent (volume ratio: 3:2), stir and dissolve, and react at 60°C for 3 hours, cool down to room temperature, concentrate and dry.
[0050] The hydrogen-containing silicone oil is IOTA203 low hydrogen-containing silicone oil (0.5 wt% hydrogen content) from Anhui Aiyota Silicone Oil Co., Ltd.; the functional monomer is trifluoroethyl methacrylate (CAS: 352-87-4) and glycidyl methacrylate (CAS: 106-91-2), the weight ratio is 0.8:1.
[0051] This example also provides a coating with good recoating performance using the above-mentioned organic silicon leveling agent. 3.
[0052] Described...
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