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A method of improving the insulation resistance value of chip capacitor

A technology of insulation resistance and capacitors, which is applied in the direction of capacitors, capacitor manufacturing, circuits, etc., can solve the problems of large differences in insulation resistance values ​​of capacitors, poor consistency, and difficult technical control, so as to improve the insulation resistance value and improve the insulation resistance. Value and consistency, the effect of simple and easy method

Inactive Publication Date: 2020-12-25
HUBEI UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] On the other hand, acceptor ions and vitrified (or insulating) substances in the grain boundary layer enter the grain boundary through thermal diffusion, but this process is extremely difficult to control precisely in technology, so in actual products, the insulation resistance value of the capacitor There are often large differences and poor consistency, which affects the stability of product use
In summary, there is no effective way to increase the insulation resistance and consistency of STO chip capacitors without reducing their capacitance, and this problem needs to be solved urgently.

Method used

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  • A method of improving the insulation resistance value of chip capacitor
  • A method of improving the insulation resistance value of chip capacitor
  • A method of improving the insulation resistance value of chip capacitor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] Load a constant voltage on the STO chip capacitor: 50V DC voltage, and at the same time rapidly heat up to 200°C at a rate of 50°C / min in the rapid annealing furnace. After 100s at this temperature, take the capacitor out of the annealing furnace and place it quickly. Rapidly cool in liquid nitrogen for 2 minutes, then take out the capacitor and let it rise to room temperature naturally in the air. After electrical and heat treatment, the insulation resistance of STO chip capacitors can be greatly increased by 10 to 30 times without changing the capacitance value, loss and capacitance temperature coefficient of the capacitor, and the resistance consistency is also improved. like image 3 Shown is the graph of the variation of insulation resistance with measurement time before and after STO chip capacitor treatment. It can be seen from the figure that after thermal and electrical treatment, the insulation resistance value of the chip capacitor rises from the original 1....

Embodiment 2

[0051] Load a constant voltage on the STO chip capacitor: 50V DC voltage, and at the same time in the rapid annealing furnace at a rate of 40°C / min, rapidly heat up to 180°C, and after 120s at this temperature, take the capacitor out of the annealing furnace and place it quickly Rapidly cool in liquid nitrogen for 1 minute, then take out the capacitor and let it rise to room temperature naturally in the air. After electrical and heat treatment, the insulation resistance of STO chip capacitors can be greatly increased by 10 to 30 times without changing the capacitance value, loss and capacitance temperature coefficient of the capacitor, and the resistance consistency is also improved.

Embodiment 3

[0053] Load a constant voltage on the STO chip capacitor: 50V DC voltage, and at the same time in the rapid annealing furnace at a rate of 60°C / min, rapidly raise the temperature to 220°C, and after 80s at this temperature, take the capacitor out of the annealing furnace and place it quickly Rapidly cool in liquid nitrogen for 3 minutes, then take out the capacitor and let it rise to room temperature naturally in the air. After electrical and heat treatment, the insulation resistance of STO chip capacitors can be greatly increased by 10 to 30 times without changing the capacitance value, loss and capacitance temperature coefficient of the capacitor, and the resistance consistency is also improved.

[0054] The above-mentioned embodiments 1-3 adopt a simple and easy physical method, that is, the STO chip capacitor is subjected to rapid heating and cooling treatment under the condition of applying voltage, and the insulation resistance and withstand voltage value of the chip capa...

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Abstract

The invention discloses a method for improving the insulation resistance value of a chip capacitor, which includes: loading a constant voltage on the chip capacitor; heating up to a preset temperature in an annealing furnace and keeping it for a preset time; placing the chip capacitor in liquid nitrogen Cool for 1-3 minutes; then take out the chip capacitor and let it rise to room temperature naturally in the air. This method utilizes the characteristic that the insulation resistance value of the STO chip capacitor increases continuously with the load voltage and time, and performs rapid heat treatment on the chip capacitor under the condition of the loaded voltage. This method is simple and easy to implement. Without changing the capacitance value, loss and capacitance temperature coefficient of the capacitor, the insulation resistance value and consistency of the STO ceramic chip are greatly improved. After removing the applied voltage and thermal conditions, the STO chip capacitor is insulated The resistance value does not decay over time.

Description

technical field [0001] The invention relates to the field of electronic information functional materials and devices, in particular to a method for increasing the insulation resistance value of a chip capacitor. Background technique [0002] Chip capacitors, also known as single-layer chip capacitors, were invented by American DLI and MDI companies in the 1970s. Due to their small size, large dielectric constant, wide application temperature range (-55°C ~ 125°C), and capacitance temperature stability High (≤±4.7%~≤±22%) and good frequency characteristics, etc., are widely used in microwave integration technology and microwave circuits. According to statistics, the global microwave components market in 2017 exceeded US$18 billion, of which chip capacitors accounted for about 25% of the market. Chip capacitors (single-layer grain boundary layer capacitors) generally use SrTiO 3 (STO) or electron-doped STO is used as the parent phase, which is made by one-step or two-step me...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01G13/00
CPCH01G13/00
Inventor 杨昌平李慧娟张木森梁世恒王瑞龙徐玲芳肖海波
Owner HUBEI UNIV
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