The invention discloses a high-
vacuum annealing process of an armored 
thermocouple and an armored wire. The high-
vacuum annealing process comprises the following steps: A, preparing a 
system and equipment; B, completing PLD 
programming (
system preparation and 
system condition completion), closing a main power supply, charging, ascending a furnace cover in place, starting a circulating water system, starting a control gas source and 
pneumatic valve system, starting an instrument and 
control system, starting a vacuum system, starting a 
rotary vane pump and starting a roots pump; C, when the conditions are met, starting a 
diffusion pump, when the vacuum degree is reached, putting into a 
heating system, keeping constant temperature for a period of time according to a heating curve, and finallycooling; and D, when the temperature reaches 50 DEG C, shutting down the furnace for material taking, and shutting down all the systems. The armored 
thermocouple and the armored wire which are subjected to high-
vacuum annealing are bright in surface and free of pits under a 
microscope, the withstand 
voltage between wires and the withstand 
voltage of a wire pair armor body can generally reach 2000V or above, the 
insulation resistance can generally reach 20 G and can reach 100 G or above to the maximum, the armored 
thermocouple and the armored wire are bent, and the armor body does not crack.