Preparation method of lobetyolin and novel use of lobetyolin in drugs and health products
A technology of tangshenoside and medicine, which is applied in the field of preparation of traditional Chinese medicine compounds
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experiment example 1
[0015] Experimental Example 1. Preparation and Separation of Codonopsis in Campanulaceae
[0016] The steps of the preparation and separation process are as follows: (1) Take dried platycodon root or stem and leaf samples, crush them through a 200-mesh sieve, extract with methanol or ethanol to obtain the extract, and concentrate under reduced pressure to obtain the extract; (2) Dilute the above extract with water , on D101 macroporous resin adsorption column chromatography, followed by elution with water and more than 70% ethanol, collecting 70% alcohol eluted part, concentrating the collected solution under reduced pressure, and freeze-drying to obtain a crude extract rich in tangshenoside; (3 ) Pass the obtained sample through a reversed-phase ODS column, and use 5%~85% methanol aqueous solution to elute with different concentrations, collect different effluents in sections, concentrate the effluents under reduced pressure, and finally recrystallize to obtain a purity of 95....
experiment example 2
[0018] Experimental Example 2. Preparation and Separation of Codonopsis Codonopsis Codonopsis
[0019] The steps of the preparation and separation process are as follows: (1) Take the dried Codonopsis pilosula root or stem leaf sample, crush it through a 200-mesh sieve, extract it with methanol or ethanol to obtain the extract, and concentrate it under reduced pressure to obtain the extract; (2) Dilute the above-mentioned extract with water. The extract was subjected to D101 macroporous resin adsorption column chromatography, followed by elution with water and more than 70% ethanol, collecting the 70% alcohol eluted part, concentrating the collected solution under reduced pressure, and freeze-drying to obtain a crude extract rich in tangshenoside; (3) Pass the obtained sample through a reverse-phase ODS column, and elute with 5%~85% methanol aqueous solution at different concentrations, collect different effluents in sections, concentrate the effluents under reduced pressure, a...
experiment example 3
[0021] Experimental example 3. Preparation and separation of tangshenoside in Codonopsis pilosula
[0022] The preparation and separation process steps are as follows: (1) Take the dried root sample of Codonopsis pilosula, crush it through a 200-mesh sieve, extract it with methanol or ethanol to obtain the extract, and concentrate it under reduced pressure to obtain the extract; (2) Dilute the above extract with water, and put it on D101 macroporous resin adsorption column chromatography, eluted with water and more than 70% ethanol in sequence, collected the 70% alcohol eluted part, concentrated the collected liquid under reduced pressure, and freeze-dried to obtain a crude extract rich in tangshenoside; (3) The obtained sample was passed through a reversed-phase ODS column, and eluted with 5%~85% methanol aqueous solution at different concentrations. Different effluents were collected in sections, concentrated under reduced pressure, and finally recrystallized to obtain Codono...
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