Method for preparing catalyst-loaded coal liquefied oil coal slurry
A technology for supporting catalysts and coal liquefied oil, which is applied in the petroleum industry, liquid carbon-containing fuels, fuels, etc., can solve the problems of poor dispersibility of catalysts, difficult to grow up, and large particle size of catalysts, so as to achieve small particles and difficult to grow up. , good dispersion effect
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[0029] In order to achieve the above object, the present invention provides a catalyst-loaded coal liquefied oil coal slurry preparation method, the method comprising the following steps:
[0030] (1) emulsifying the iron salt aqueous solution with the first solvent oil to obtain an iron salt homogeneous emulsion; emulsifying the alkaline aqueous solution with the second solvent oil to obtain an alkaline homogeneous emulsion;
[0031] (2) After homogeneously mixing iron salt homogeneous emulsion and oil-coal slurry, add alkaline homogeneous emulsion;
[0032] (3) The alkaline substance in the alkaline homogeneous emulsion and the iron salt in the iron salt homogeneous emulsion undergo a precipitation reaction to obtain iron hydroxide, and then pass through an oxidant to undergo an oxidation reaction to generate nano-scale iron-based Catalyst particles;
[0033] (4) After the oxidation reaction finishes, feed nitrogen, add sulfur, keep the slight positive pressure of the nitro...
Embodiment 1
[0063] Ferrous sulfate aqueous solution and the first solvent oil (anthracene oil and washing oil hydrogenated oil three times) are emulsified in the iron salt emulsification homogenization tank 1, and the emulsification temperature is 50 ° C; ammonia water and the second solvent oil (anthracene oil and washing oil three times hydrogenated oil) in the alkaline solution emulsification homogeneous tank 2 for emulsification, and the emulsification temperature is 50°C; the ferrous sulfate homogeneous emulsion is introduced into the oil-coal slurry preparation tank 3, and prepared with the oil-coal slurry The oil-coal slurry in the tank 3 was homogeneously mixed for 30 minutes; the ammonia water homogeneous emulsion was introduced into the oil-coal slurry preparation tank 3, and the ammonia water in the ammonia water homogeneous emulsion and the ferrous sulfate in the ferrous sulfate homogeneous emulsion produced Precipitation reaction, the pH value is 7, and the reaction time is 30...
Embodiment 2
[0065] The ferrous nitrate aqueous solution and the first solvent oil (anthracene oil and washing oil three times hydrogenated oil) are emulsified in the iron salt emulsification homogenization tank 1, and the emulsification temperature is 20 ° C; ammonia water and the second solvent oil (anthracene oil and washing oil three times hydrogenated oil) in the alkaline solution emulsification homogeneous tank 2 for emulsification, and the emulsification temperature is 20°C; the ferrous nitrate homogeneous emulsion is introduced into the oil-coal slurry preparation tank 3, and prepared with the oil-coal slurry The oil-coal slurry in the tank 3 was homogeneously mixed for 50 minutes; the ammonia water homogeneous emulsion was introduced into the oil-coal slurry preparation tank 3, and the ammonia water in the ammonia water homogeneous emulsion and the ferrous nitrate in the ferrous nitrate homogeneous emulsion produced Precipitation reaction, the pH value is 8.5, and the reaction time...
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