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Continuous multi-step thermal hydrogen treatment process for improving room-temperature plasticity of TC4 titanium alloy

A treatment process, titanium alloy technology, applied in the field of titanium alloy heat treatment process, can solve the problems of difficult control of microstructure and properties, high requirements for molds and forming equipment, and difficult processing, so as to reduce the investment in processing links and packaging equipment , improve efficiency and reduce difficulty

Active Publication Date: 2019-10-08
HEFEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although titanium alloys have good plastic forming properties at high temperatures, high temperatures also bring a series of problems to forming: high deformation temperature, large flow stress, difficult control of microstructure and properties, and high requirements for molds and forming equipment
However, for hydrogen-absorbing titanium alloy samples with large volume and mass, the vacuum packaging and solution quenching treatment are more difficult.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Step 1. After the TC4 titanium alloy sample is polished with sandpaper, it is ultrasonically cleaned in absolute ethanol, and then dried to ensure that the surface of the sample is free of pollution;

[0025] Step 2. Put the sample into the furnace tube of the tube furnace, turn on the vacuum system, and evacuate until the vacuum degree in the furnace tube is lower than 1.5×10 -3 Pa; start to heat up at a rate of 10°C / min, and close the vacuum valve at the end of the vacuum system when the temperature rises to 750°C;

[0026] Step 3. Fill the furnace tube with hydrogen to -0.08MPa and keep it warm for 1 hour. The number of hydrogen filling steps at this time is recorded as 1 step;

[0027] Step 4. After the heat preservation in the previous step, fill the furnace tube with hydrogen again. In this step, fill the hydrogen with 0.008MPa, keep the heat for 1 hour, and the number of hydrogen filling steps +1;

[0028] Step 5. Repeat step 4 until the number of hydrogen charg...

Embodiment 2

[0031] Step 1. After the TC4 titanium alloy sample is polished with sandpaper, it is ultrasonically cleaned in absolute ethanol, and then dried to ensure that the surface of the sample is free of pollution;

[0032] Step 2. Put the sample into the furnace tube of the tube furnace, turn on the vacuum system, and evacuate until the vacuum degree in the furnace tube is lower than 1.5×10 -3 Pa; start to heat up at a rate of 10°C / min, and close the vacuum valve at the end of the vacuum system when the temperature rises to 800°C;

[0033] Step 3. Fill the furnace tube with hydrogen to -0.08MPa and keep it warm for 1 hour. The number of hydrogen filling steps at this time is recorded as 1 step;

[0034] Step 4. After the heat preservation in the previous step, fill the furnace tube with hydrogen again. In this step, fill the hydrogen with 0.008MPa, keep the heat for 1 hour, and the number of hydrogen filling steps +1;

[0035] Step 5. Repeat step 4 until the number of hydrogen charg...

Embodiment 3

[0038] Step 1. After the TC4 titanium alloy sample is polished with sandpaper, it is ultrasonically cleaned in absolute ethanol, and then dried to ensure that the surface of the sample is free of pollution;

[0039] Step 2. Put the sample into the furnace tube of the tube furnace, turn on the vacuum system, and evacuate until the vacuum degree in the furnace tube is lower than 1.5×10 -3 Pa; start to heat up at a rate of 10°C / min, and close the vacuum valve at the end of the vacuum system when the temperature rises to 850°C;

[0040] Step 3. Fill the furnace tube with hydrogen to -0.08MPa and keep it warm for 1 hour. The number of hydrogen filling steps at this time is recorded as 1 step;

[0041] Step 4. After the heat preservation in the previous step, fill the furnace tube with hydrogen again. In this step, fill the hydrogen with 0.008MPa, keep the heat for 1 hour, and the number of hydrogen filling steps +1;

[0042] Step 5. Repeat step 4 until the number of hydrogen charg...

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PUM

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Abstract

The invention discloses a continuous multi-step thermal hydrogen treatment process for improving room-temperature plasticity of a TC4 titanium alloy. The process comprises the steps of performing surface treatment on a TC4 titanium alloy sample, heating the sample in a vacuum environment to a hydrogen filling temperature, performing continuous multi-step hydrogen filling, performing heat preservation to a stable hydrogen pressure at least after per step of hydrogen filling, and performing air cooling to a room temperature after the final-step hydrogen filling to complete the improvement of theroom-temperature plasticity of the TC4 titanium alloy. The process is simple and convenient in method, low in cost and obvious in plasticization effect; the room-temperature plasticity of the treatedTC4 titanium alloy is obviously improved; the room-temperature plasticity forming of a TC4 titanium alloy complex structure part is facilitated; and an application scope of the TC4 titanium alloy canbe expanded.

Description

technical field [0001] The invention belongs to the field of titanium alloy material processing, and in particular relates to a titanium alloy heat treatment process. Background technique [0002] At present, titanium alloys are widely used in aviation, aerospace and other fields due to a series of excellent properties such as high specific strength, good high temperature resistance, good corrosion resistance, and non-magnetic properties. TC4 titanium alloy is an α+β type titanium alloy with good comprehensive properties, and is the most widely used titanium alloy at home and abroad. However, TC4 titanium alloy has low plasticity and low deformation limit at room temperature, and it is easy to crack during cold forming, which limits its plastic forming at room temperature. At present, most titanium alloys need plastic forming at high temperature. Although titanium alloys have good plastic forming properties at high temperatures, high temperatures also bring a series of pro...

Claims

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Application Information

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IPC IPC(8): C22F1/18
CPCC22F1/183
Inventor 袁宝国杜江飞陈强张小雪
Owner HEFEI UNIV OF TECH
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