Continuous multi-step thermal hydrogen treatment process for improving room-temperature plasticity of TC4 titanium alloy
A treatment process, titanium alloy technology, applied in the field of titanium alloy heat treatment process, can solve the problems of difficult control of microstructure and properties, high requirements for molds and forming equipment, and difficult processing, so as to reduce the investment in processing links and packaging equipment , improve efficiency and reduce difficulty
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Embodiment 1
[0024] Step 1. After the TC4 titanium alloy sample is polished with sandpaper, it is ultrasonically cleaned in absolute ethanol, and then dried to ensure that the surface of the sample is free of pollution;
[0025] Step 2. Put the sample into the furnace tube of the tube furnace, turn on the vacuum system, and evacuate until the vacuum degree in the furnace tube is lower than 1.5×10 -3 Pa; start to heat up at a rate of 10°C / min, and close the vacuum valve at the end of the vacuum system when the temperature rises to 750°C;
[0026] Step 3. Fill the furnace tube with hydrogen to -0.08MPa and keep it warm for 1 hour. The number of hydrogen filling steps at this time is recorded as 1 step;
[0027] Step 4. After the heat preservation in the previous step, fill the furnace tube with hydrogen again. In this step, fill the hydrogen with 0.008MPa, keep the heat for 1 hour, and the number of hydrogen filling steps +1;
[0028] Step 5. Repeat step 4 until the number of hydrogen charg...
Embodiment 2
[0031] Step 1. After the TC4 titanium alloy sample is polished with sandpaper, it is ultrasonically cleaned in absolute ethanol, and then dried to ensure that the surface of the sample is free of pollution;
[0032] Step 2. Put the sample into the furnace tube of the tube furnace, turn on the vacuum system, and evacuate until the vacuum degree in the furnace tube is lower than 1.5×10 -3 Pa; start to heat up at a rate of 10°C / min, and close the vacuum valve at the end of the vacuum system when the temperature rises to 800°C;
[0033] Step 3. Fill the furnace tube with hydrogen to -0.08MPa and keep it warm for 1 hour. The number of hydrogen filling steps at this time is recorded as 1 step;
[0034] Step 4. After the heat preservation in the previous step, fill the furnace tube with hydrogen again. In this step, fill the hydrogen with 0.008MPa, keep the heat for 1 hour, and the number of hydrogen filling steps +1;
[0035] Step 5. Repeat step 4 until the number of hydrogen charg...
Embodiment 3
[0038] Step 1. After the TC4 titanium alloy sample is polished with sandpaper, it is ultrasonically cleaned in absolute ethanol, and then dried to ensure that the surface of the sample is free of pollution;
[0039] Step 2. Put the sample into the furnace tube of the tube furnace, turn on the vacuum system, and evacuate until the vacuum degree in the furnace tube is lower than 1.5×10 -3 Pa; start to heat up at a rate of 10°C / min, and close the vacuum valve at the end of the vacuum system when the temperature rises to 850°C;
[0040] Step 3. Fill the furnace tube with hydrogen to -0.08MPa and keep it warm for 1 hour. The number of hydrogen filling steps at this time is recorded as 1 step;
[0041] Step 4. After the heat preservation in the previous step, fill the furnace tube with hydrogen again. In this step, fill the hydrogen with 0.008MPa, keep the heat for 1 hour, and the number of hydrogen filling steps +1;
[0042] Step 5. Repeat step 4 until the number of hydrogen charg...
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