Adhesive tape, article, motor and manufacturing method of article
An adhesive tape and bonding technology, which is applied in the direction of bonding method, adhesive, and adhesive type using foam adhesives, which can solve the problem of adhesive tape bonding position offset, no initial adhesion, Problems such as low initial adhesion on the surface of the adhesive tape to achieve the effect of excellent adhesive strength
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preparation example 1
[0085]
[0086] By adding 7.0 parts by mass of epoxy resin 1 (epoxy equivalent of 403g / eq., liquid (25°C), viscosity of 1.4 million mPa·s (25°C)), epoxy resin 2 (epoxy equivalent of 162g / eq ., solid state (25°C), melt viscosity at 150°C is 0.2dPa·s, softening point is 25°C) 28 parts by mass, epoxy resin 3 (epoxy equivalent is 8000g / eq., solid state (25°C), 216.7 parts by mass of a methyl ethyl ketone solution (30% by mass of solid content) with a softening point of 200°C or higher, a curing agent (2,4-diamino-6-[2'-methylimidazolyl-(1')]-ethyl base-secondary triazine isocyanuric acid adduct) 2.0 parts by mass were mixed to prepare a thermosetting adhesive composition (a-1).
preparation example 2
[0088] Change epoxy resin 1 from 7 parts by mass to 2 parts by mass, and use 5 parts by mass of epoxy resin 4 (epoxy equivalent: 130g / eq., liquid (25°C), viscosity: 300mPa·s (25°C)), Other than that, the thermosetting adhesive composition (a-2) was obtained by the method similar to preparation example 1.
preparation example 3
[0090]
[0091] In a reaction vessel equipped with a stirrer, a reflux condenser, a thermometer, a dropping funnel, and a nitrogen inlet, 80 parts by mass of butyl acrylate, 15 parts by mass of acrylic acid, 5 parts by mass of hydroxyethyl acrylate, and 2 as a polymerization initiator, An acrylic copolymer (S-1) solution having a weight average molecular weight of 1 million was obtained by dissolving 0.1 parts by mass of 2'-azobisisobutyronitrile in 100 parts by mass of ethyl acetate and polymerizing at 70° C. for 10 hours.
[0092]Next, to the above-mentioned acrylic copolymer (S-1) solution, 10 parts by mass of an epoxy-based crosslinking agent ("E-05X" manufactured by Soken Chemical Co., Ltd., Solid content: 0.5 mass %), ethyl acetate was added, and it stirred for 20 minutes, and the pressure-sensitive-adhesive composition (b-1) whose nonvolatile matter was 30 mass % was obtained.
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