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Method for preparing porous polyvinylidene fluoride super-hydrophobic coating layer

A technology of polyvinylidene fluoride and super-hydrophobic coating, applied in the direction of coating, etc., can solve the problems of complicated manufacturing process and long cycle, and achieve the effect of simple process, strong anti-icing ability and good application prospect

Active Publication Date: 2019-12-13
国家能源集团龙源江永风力发电有限公司
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Problems solved by technology

[0004] At present, the methods for preparing superhydrophobic coatings include: sol-gel method, plasma fluorination method, electrospinning method, etc. However, although the coatings prepared by these methods are effective, the manufacturing process is complicated and the cycle is long. Long, for equipment with a large demand such as fan blades, the requirements for the preparation methods of the existing superhydrophobic coatings, therefore, how to prepare fan blades in a simple, convenient, low-cost, high-efficiency, large-scale The super-hydrophobic coating is very important for improving the performance and power generation of wind turbines

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  • Method for preparing porous polyvinylidene fluoride super-hydrophobic coating layer

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Embodiment 1

[0031] A preparation method for a porous polyvinylidene fluoride superhydrophobic coating, comprising the following steps:

[0032] S1. According to the mass ratio of polyvinylidene fluoride and N,N-dimethylformamide is 1:10, polyvinylidene fluoride (PVDF powder, industrial grade white fine powder) and N,N-dimethylformamide Amides were mixed and stirred for 30 minutes at a temperature of 50°C and a rotational speed of 600r / min, so that the polyvinylidene fluoride was uniformly dissolved in N,N-dimethylformamide to obtain a uniform transparent solution.

[0033] S2. According to the mass percentage of perfluorodecyltriethoxysilane in the porous polyvinylidene fluoride superhydrophobic coating is 3%, perfluorodecyltriethoxysilane is mixed with the transparent solution obtained in step S1, Stir for 20 minutes to obtain a mixed solution of perfluorodecyltriethoxysilane.

[0034] S3, according to the mass percent of the composite nano-titanium dioxide particles in the porous polyv...

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Abstract

The invention discloses a method for preparing a porous polyvinylidene fluoride super-hydrophobic coating layer. The method comprises the following steps: mixing polyvinylidene fluoride and N,N-dimethyl formamide, performing stirring, mixing the obtained transparent solution with perfluordecyl triethoxy silane, performing stirring, mixing the obtained perfluordecyl triethoxy silane mixed solutionwith composite nano titanium dioxide granules, performing stirring, performing ultrasonic treatment, and smearing or spraying the obtained porous polyvinylidene fluoride super-hydrophobic coating to asubstrate, so as to obtain a porous polyvinylidene fluoride super-hydrophobic coating layer. The method disclosed by the invention has the advantages of being simple in process, convenient to operate, cheap in raw material, easy in industrial production, and the like, and the super-hydrophobic coating layer which is excellent in super-hydrophobic performance, good in ice resistance and wind resistance, good in weather resistance and good in adaptability can be prepared in a large scale, can be widely applied to anti-ice treatment on fan blades, has great significances for improving the performance and increasing the power generation capacity of a wind turbine generator, and has high use value and good application prospects.

Description

technical field [0001] The invention belongs to the technical field of super-hydrophobic coatings, and relates to a method for preparing a porous polyvinylidene fluoride super-hydrophobic coating. Background technique [0002] In recent years, natural energy resources such as coal and oil have been decreasing due to the large amount of energy resources consumed in industry and daily life. In order to solve the energy crisis, wind power projects have attracted much attention. In a wind power generation system, wind turbine blades are an important part of obtaining wind energy. However, wind turbine blades exposed to cold climates are often found to develop icing. Ice that forms on wind turbine blades can cause serious problems if not removed in time. [0003] In order to ensure the maximum reliability of wind turbine blades and reduce economic losses caused by icing, there are currently the following two methods to reduce or eliminate the phenomenon of ice accumulation on ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D127/16C09D7/63C09D7/61
CPCC08K2003/2241C08K2201/011C08K2201/014C09D127/16C09D7/61C09D7/63C08K5/5419C08K3/22
Inventor 王训达王瑞丰段焱森何建军陈标周承伟揭军鲍江涌罗金
Owner 国家能源集团龙源江永风力发电有限公司
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