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A wear-resistant anti-reflection coating system for coating surface and preparation method thereof

A wear-resistant coating and wear-resistant coating technology, which is applied in the field of wear-resistant and anti-reflection coating system for coating surface and its preparation, can solve the problem of no reports of wear-resistant anti-reflection protective coatings for transparent parts, and achieve good transparency. Effect

Active Publication Date: 2021-07-09
中昊北方涂料工业研究设计院有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, there are many kinds of coatings for transparent parts and transparent parts wear-resistant protection, but there is no report on the wear-resistant and anti-reflection protective coatings for transparent parts with double-sided coating.

Method used

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  • A wear-resistant anti-reflection coating system for coating surface and preparation method thereof
  • A wear-resistant anti-reflection coating system for coating surface and preparation method thereof
  • A wear-resistant anti-reflection coating system for coating surface and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0028] Preparation of coating A: 90 g of methyl triethoxysilane was added to the reactor, and 45 g is proprof aluminum aluminum is uniform, and the mixture is cooled to 0 ° C by ice salt bath, and 3 g of hydrochloric acid and 25 g of distilled water are mixed. In the above reactor, the mixture of methyltrutinethoxysilane and isopropanol aluminum is rapidly mixed under stirring, and then the stirring reaction is continued in the ice salt bath, first add 35 g of silica sol, then add 8 g. Ethanol, temperature rise makes the system reflux, reflux 0.5 to 2 hours, 20 g of diazone alcohol, 1 g of QE-340M and 12G γ- (2,3-cyclopproxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxoxy). A-1 after cooling. .

Embodiment 2

[0030] Preparation of coating A: 90 g of methyl triethoxysilane was added to the reactor, 60 g of isopropanol aluminum aluminum was mixed, and the mixture was cooled to 0 ° C below 0 ° C, 3 g of hydrochloric acid and 25 g of distilled water were mixed and uniform. In the above reactor, the mixture of methyltriethoxysilane and isopropanol aluminum is rapidly mixed under stirring, and then the stirring reaction is continued in the ice salt bath for 2 to 4 hours, then add 35 g of silica sol, and then add 5g. Normal propyl alcohol, the temperature increases the system reflux, refluxed 0.5 ~ 2 hours, cooling 25 g of diazone alcohol, 2G trimethylolpropane three (2-mercaptoacetate) and 15Gγ- (2,3-epoxy) Oxygen) propyltrimethoxysilane gives coating A-2.

Embodiment 3

[0032] Preparation of coating A: 110 g of phenyltriethoxysilane, 45 g of isopropanol aluminum, 20 g of positive propanol zirconium aluminum, 20 g of positive propanol zirconia, cooled to 0 ° C below 0 ° C, 3 g of hydrochloric acid and 34g When the distilled water is mixed, it is rapidly added to the above reactor and rapidly mixed with phenyltriethoxysilane, isopropanol aluminum and n-propoxyzine mixture under stirring, and continues to be stirred in the ice salt bath for 2 to 4 hours. Add 25G silica sol, temperature rise to reflux the system, reflow 0.5 ~ 2 hours, 50 g of dipropyl alcohol, 2 g of QE-340M and 15G γ- (2,3-cyclopionoxy) propyltrimethoxysilane to obtain coatings A-3.

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Abstract

The invention relates to the technical field of anti-reflection coatings, in particular to a wear-resistant anti-reflection coating system for coating surfaces and a preparation method thereof. The coating system of the present invention is composed of two kinds of coating materials, which are respectively coated on the front and back sides of the coated transparent parts. , the opposite side facing away from the optical path, adopts a transparent wear-resistant coating with a low refractive index, and the corresponding coating is B. If A coating or B coating is used at the same time on the front and back, the anti-reflection effect cannot be achieved.

Description

Technical field [0001] The present invention relates to the field of increasing coating, and more particularly to a wear-resistant and increasing coating system with a coating surface and a preparation method thereof. Background technique [0002] Organic glass (PMMA) and polycarbonate (PC) transparent applications are increasingly wide, with the needs of special functions, they need to be plated with their surface, these coating mainly have gold film, silver film, indium tin oxide, tin oxide Zinc oxide, etc., such coating wear resistance does not meet the actual use requirements, and some of the light transmittances are poor, except for the transparent parts of single-sided coating, many coating transparenses need double-sided sides due to actual use requirements The glass-plated, the transparent parts of the double-sided coating have further decreased. Therefore, it is necessary to develop transparent wear-resistant protective coatings, which should have good wear resistance, l...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D183/04C09D183/08C09D7/61C09D7/63
CPCC08G77/04C08G77/24C09D4/00C09D183/04C09D183/08C09D7/61C09D7/63C08K3/36C08K5/5435C08K5/37
Inventor 王志强魏超顾剑东李斌施颖波周敏
Owner 中昊北方涂料工业研究设计院有限公司