A kind of preparation method and application of nb-mo eutectic mesoporous metal oxide catalyst
A technology of oxides and catalysts, applied in the direction of metal/metal oxide/metal hydroxide catalysts, preparation of organic compounds, physical/chemical process catalysts, etc., can solve the problems of large catalyst differences and low catalyst repeatability, Achieve the effects of simple preparation method, short preparation cycle and high catalytic activity
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Embodiment 1
[0036] Embodiment 1: Provide a kind of Nb 0.8 Mo 0.2 O x Catalyst preparation method
[0037] a) 7.5g cetyltrimethylammonium bromide is dissolved in 7.5mL H 2 In O, stir at 40°C until completely dissolved. Recorded as A solution.
[0038] b) Weigh 8mmol NbCl 5 (2.161g) and 2mmol MoCl 5 (0.546g), gradually added to 10mL ethanol solution, stirring vigorously for about 10min. Recorded as B solution.
[0039] c) Add B solution to A solution dropwise, and further fully stir for about 30 minutes. This solution is referred to as C solution.
[0040] d) Prepare 10 mL of HCl aqueous solution with pH ≈ 1, and add it to C solution. This solution is referred to as D solution.
[0041] e) Transfer D solution to a hydrothermal kettle and hydrothermally heat it at 160°C for 24 hours.
[0042] f) After the hydrothermal kettle is lowered to room temperature, the product in the kettle is washed to neutrality, and the solid product is separated by suction filtration.
[0043] g) Place the solid product ...
Embodiment 2
[0045] Embodiment 2: Provide a kind of Nb 0.5 Mo 0.5 O x Catalyst preparation method
[0046] Take 5mmol NbCl in step (b) 5 (1.351g) and 5mmol MoCl 5 (1.366g) was dissolved in ethanol and stirred well to prepare B solution. The remaining steps are the same as in Example 1.
Embodiment 3
[0047] Embodiment 3: Provide a kind of Nb 0.2 Mo 0.8 O x Catalyst preparation method
[0048] Take 2mmol NbCl in step (b) 5 (0.540g) and 8mmol MoCl 5 (2.186g) was dissolved in ethanol and stirred well to prepare B solution. The remaining steps are the same as in Example 1.
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