Preparation method of corrosion-resistant chemical barrel material
A corrosion-resistant and chemical technology, which is applied in the field of preparation of corrosion-resistant chemical barrel materials, can solve problems such as being unable to withstand high-temperature erosion, and achieve the effects of maintaining stable chemical properties, improving corrosion resistance, and wear-resistant relative density
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Embodiment 1
[0013] A method for preparing a corrosion-resistant chemical barrel material, comprising the following steps:
[0014] S1: Preparation of nano-ceramic materials: Weigh 8.5 grams of silicon nitride and 4.0 grams of graphite powder, mix and grind them for 20 minutes, place them in a beaker, add 20 milliliters of titanium dioxide hydrogel into the beaker, disperse them ultrasonically for 10 minutes, and then add them to the dispersion Add 50 ml of ethylene glycol aqueous solution to the mixture, mix at high speed for 30 minutes at 1000 rpm, let it stand in an oven at 70°C for 4 hours, and then send it into a muffle furnace for calcination for 3 hours at a calcination temperature of 800°C, and cool with the furnace To normal temperature, it can be ground into powder; wherein, the mass concentration of titanium dioxide in the titanium dioxide hydrogel is 28%, and the mass concentration of the ethylene glycol aqueous solution is 60%. The nano-ceramic material prepared by the inventi...
Embodiment 2
[0018] A method for preparing a corrosion-resistant chemical barrel material, comprising the following steps:
[0019] S1: Preparation of nano-ceramic materials: 8.8 grams of silicon nitride and 4.2 grams of graphite powder were mixed and ground for 25 minutes in turn, placed in a beaker, 22 milliliters of titanium dioxide hydrogel was added to the beaker, ultrasonically dispersed for 12 minutes, and then added to the dispersion Add 55 ml of ethylene glycol aqueous solution, mix at 1100 rpm for 35 minutes at high speed, let it stand in an oven at 75°C for 5 hours, then put it into a muffle furnace for calcination for 3.5 hours, the calcination temperature is 850°C, and cool with the furnace To normal temperature, it can be ground into powder; wherein, the mass concentration of titanium dioxide in the titanium dioxide hydrogel is 29%, and the mass concentration of the ethylene glycol aqueous solution is 62%. The nano-ceramic material prepared by the invention has phase transiti...
Embodiment 3
[0023] A method for preparing a corrosion-resistant chemical barrel material, comprising the following steps:
[0024]S1: Preparation of nano-ceramic materials: Weigh 9.0 grams of silicon nitride and 4.5 grams of graphite powder, mix and grind for 30 minutes, put them in a beaker, add 24 milliliters of titanium dioxide hydrogel into the beaker, ultrasonically disperse for 15 minutes, and then add Add 60 ml of ethylene glycol aqueous solution to the mixture, mix at 1200 rpm for 40 minutes at high speed, let it stand in an oven at 80°C for 6 hours, then send it to a muffle furnace for calcination for 4 hours at a temperature of 900°C, and cool with the furnace To normal temperature, it can be ground into powder; wherein, the mass concentration of titanium dioxide in the titanium dioxide hydrogel is 30%, and the mass concentration of the ethylene glycol aqueous solution is 65%. The nano-ceramic material prepared by the invention has phase transition toughness, particle size betwe...
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