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Preparation method of dendrobium aurantiacum powder

A technology for stacking dendrobium and dendrobium tablets, which is applied in the directions of non-active ingredients medical preparations, medical preparations containing active ingredients, powder delivery, etc. Strong inhibitory effect, improving extraction rate and gypsum rate, and improving solubility

Active Publication Date: 2020-02-07
贵州天诚农业科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The method provided by the above-mentioned patent reduces the loss rate of active ingredients in Dendrobium, but the solubility of active ingredients in Dendrobium powder is small, and the bioabsorption and availability are still low

Method used

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  • Preparation method of dendrobium aurantiacum powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A preparation method of dendrobium sheath powder, comprising the following steps:

[0028] (1) Cleaning treatment: Remove the leaves of fresh Dendrobium sheathing, put them in the cleaning solution and soak them for 6 minutes, then take them out and send them to the dehydrator to remove the moisture on the surface, and set aside:

[0029] (2) Drying: send the dehydrated Dendrobium sheaths to a hot air circulation oven, dry at 50-60°C until the water content is 60-70%, and then cut into dendrobium slices;

[0030] (3) freezing treatment: freezing the dendrobium sheet at -15°C for 20h;

[0031] (4) differential pressure puffing treatment: adding the frozen dendrobium slices into the puffing tank and carrying out pressure differential puffing to obtain puffed dendrobium slices;

[0032] (5) Low-temperature reflux extraction and concentration: add the expanded Dendrobium flakes to a hot reflux low-temperature extraction low-temperature concentrator, add an organic solvent ...

Embodiment 2

[0042] A preparation method of dendrobium sheath powder, comprising the following steps:

[0043] (1) Cleaning treatment: remove the leaves of fresh Dendrobium sheathing, put them in the cleaning solution and soak them for 8 minutes, then take them out and send them to the dehydrator to remove the moisture on the surface, and set aside:

[0044](2) Drying: send the dehydrated Dendrobium sheaths to a hot air circulation oven, dry at 50-60°C until the water content is 60-70%, and then cut into dendrobium slices;

[0045] (3) freezing treatment: freezing the dendrobium sheet at -18°C for 15h;

[0046] (4) differential pressure puffing treatment: adding the frozen dendrobium slices into the puffing tank and carrying out pressure differential puffing to obtain puffed dendrobium slices;

[0047] (5) Low-temperature reflux extraction and concentration: add the expanded Dendrobium flakes to a heat reflux low-temperature extraction low-temperature concentrator, add an organic solvent ...

Embodiment 3

[0057] A preparation method of dendrobium sheath powder, comprising the following steps:

[0058] (1) Cleaning treatment: Remove the leaves of fresh Dendrobium sheathing, put them in the cleaning solution and soak them for 8 minutes, then take them out and send them to the dehydrator to remove the moisture on the surface, and set aside:

[0059] (2) Drying: send the dehydrated Dendrobium sheaths to a hot air circulation oven, dry at 50-60°C until the water content is 60-70%, and then cut into dendrobium slices;

[0060] (3) freezing treatment: freezing the dendrobium sheet at -18°C for 20h;

[0061] (4) differential pressure puffing treatment: adding the frozen dendrobium slices into the puffing tank and carrying out pressure differential puffing to obtain puffed dendrobium slices;

[0062] (5) Low-temperature reflux extraction and concentration: add the expanded Dendrobium flakes to a heat reflux low-temperature extraction low-temperature concentrator, add an organic solvent...

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Abstract

The invention relates to a preparation method of dendrobium aurantiacum powder. The preparation method comprises the following steps of (1) performing cleaning treatment: removing leaves of fresh dendrobium aurantiacum, adding the dendrobium aurantiacum without leaves in cleaning liquid, performing soaking and cleaning, performing fishing out, and removing surface moisture for standby application;(2) performing drying: drying the dehydrated dendrobium aurantiacum until the water content is 60-70%, and performing cutting into slices; (3) performing freezing treatment: freezing the dendrobium aurantiacum slices; (4) performing differential pressure puffing treatment: performing differential pressure puffing on the frozen dendrobium aurantiacum slices, to prepare the puffed dendrobium aurantiacum slices; (5) performing low-temperature reflow extraction and concentration: adding an organic solvent to the puffed dendrobium aurantiacum slices, and performing low-temperature reflow extraction and concentration to prepare primary concentrate; (6) performing concentration: sending primary concentrate into a spherical vacuum concentrating tank, and performing concentration to prepare secondary concentrate; (7) performing drying and crushing: drying a secondary concentrated solution, and performing crushing, to prepare crude dendrobium aurantiacum powder; and (8) preparing components. According to the method provided by the invention, the bioactive components of the dendrobium aurantiacum are low in loss rate, high in dissolving and leaching efficiency and high in biology absorptionand utilization rate.

Description

technical field [0001] The invention belongs to the technical field of medicinal material extraction, and in particular relates to a preparation method of dendrobium sheathing dendrobium powder. Background technique [0002] Dendrobium dendrobii is a variety of Dendrobium lanceolata, which is mainly distributed in the southwest of Sichuan Province, the southwest to northwest of Guangxi, the south of Guizhou, and the southeast of Yunnan. At present, it is widely cultivated and used for medicinal purposes in Jiajiang County, Leshan City, Sichuan Province. The difference between Dendrobium sheathing and the original variety is that the plant is obviously thicker, the stem is more than 4 mm thick, the leaves are 1.8-4.5 cm wide, the inflorescences are 5-14 cm long, the bracts are 1.8-3 cm long, and there is a big purple on the lip. plaque. Dendrobium dendrobii mainly contains polysaccharides, tannins, bibenzyls, alkaloids, coumarins, sugars, glycosides, phenanthrenes, fluoreno...

Claims

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Application Information

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IPC IPC(8): A61K36/8984A61K9/14A61K47/38
CPCA61K9/146A61K36/8984A61K2236/10A61K2236/13A61K2236/17A61K2236/19A61K2236/333A61K2236/51
Inventor 周高飞吴文伟
Owner 贵州天诚农业科技发展有限公司
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