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Quadruple-effect solvent recovery energy-saving system and method

An energy-saving system and solvent technology, applied in chemical instruments and methods, multi-effect evaporation, chemical industry, etc., can solve the problems of increasing energy consumption of salt recovery, affecting distillation effect, and large amount of waste water, so as to avoid foaming and ensure Distillation effect, the effect of reducing the amount of salty waste liquid

Pending Publication Date: 2020-02-28
肥城金塔酒精化工设备有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, in the recovery of alcohol, the two mother liquors are generally mixed and then distilled and recovered together. There are many problems in this distillation method: ① In order to ensure a good distillation recovery effect, multi-effect distillation is generally required. In order to achieve multi-effect distillation, in a In high-efficiency distillation, the temperature is generally higher, and the higher distillation temperature will cause the first mother liquor in the mixed liquor to foam and affect the distillation effect; ②The second mother liquor contains salt, and the salty wastewater produced after distillation needs to be evaporated The system recovers salt. The first mother liquor does not contain salt, and the wastewater generated after distillation is directly sent to the wastewater treatment system. The mixed distillation of the two mother liquors produces a large amount of wastewater, which increases the energy consumption of subsequent salt recovery.

Method used

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  • Quadruple-effect solvent recovery energy-saving system and method

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Effect test

Embodiment 1

[0033] Such as figure 1 As shown, the four-effect solvent recovery energy-saving system includes a first-effect recovery tower 1, a second-effect recovery tower 2, a three-effect recovery tower 3, a four-effect recovery tower 4, a first-effect evaporation tower 5, a second-effect evaporation tower 6, and a three-effect evaporation tower 7. The first mother liquor raw material tank 8 and the second mother liquor raw material tank 9 .

[0034]The first mother liquor raw material tank 8 is connected to the inlet end of the four-effect recovery tower 4 through the four-effect recovery feed preheater 31 through the pipeline, and the outlet end of the four-effect recovery tower 4 tower top is connected to the condenser group 10 through the pipeline. The inlet end is connected, the outlet end of the condenser group 10 is connected with the vacuum pump system 20 through the pipeline, and the outlet end of the condenser group 10 is also connected with the four-effect tower product tank...

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Abstract

The invention discloses a quadruple-effect solvent recovery energy-saving system. The system comprises a first-effect recovery tower, a second-effect recovery tower, a third-effect recovery tower, a fourth-effect recovery tower, a first-effect evaporation tower, a second-effect evaporation tower, a third-effect evaporation tower, a first mother liquor raw material tank and a second mother liquor raw material tank. The method for recovering alcohol by using the system comprises the following steps: separately distilling the first mother liquor and the second mother liquor, and carrying out low-temperature distillation on the first mother liquor foamed by high-temperature distillation through the fourth-effect recovery tower and the third-effect recovery tower and distilling the second mother liquor which does not foam after high-temperature distillation through the first-effect evaporator, the first-effect recovery tower, the second-effect evaporation tower, the second-effect recovery tower, the third-effect evaporation tower and the third-effect recovery tower. Foaming in the distillation process is avoided, and meanwhile, the energy consumption in post-treatment on the waste liquid is reduced.

Description

technical field [0001] The invention relates to the technical field of alcohol recovery, in particular to a four-effect solvent recovery energy-saving system and method. Background technique [0002] At present, the alcohol content of the waste liquid after the alcohol extraction section is generally 50%-55%, and alcohol needs to be recovered through the alcohol recovery section. During alcohol recovery, the waste liquid with an alcohol content of 50%-55% is used as the mother liquor. At present, the mother liquor generally includes two types. The first mother liquor comes from the purification section of the alcohol extraction process, which contains water, ethanol and a large amount of organic matter, of which the organic matter content is about 1%, and it is easy to foam when distilled at a higher temperature; the second mother liquor This kind of mother liquor comes from the refining section of the alcohol extraction process. It contains water, ethanol, salt and a small ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D1/26B01D1/30C07C29/80C07C31/08
CPCB01D1/26B01D1/30C07C29/80C07C31/08Y02P20/10Y02P20/50Y02P70/10
Inventor 赵守合田浩王坤陈红霞刘英云邱金月孙彦彬王芳李建图
Owner 肥城金塔酒精化工设备有限公司
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