Unlock instant, AI-driven research and patent intelligence for your innovation.

Method for preparing bio-based composite material by using palm biomass powder as raw material

A biomass powder and composite material technology, which is applied in separation methods, chemical instruments and methods, sedimentation tanks, etc., can solve the problems affecting the durability of finished products, high nutrient content, and biological damage to finished products, and reduce environmental protection. The effect of pressure, high performance, good processability

Pending Publication Date: 2020-03-24
LIAONING XINGFUREN TECH CO LTD +1
View PDF5 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At the same time, the nutrient content in palm residue is high, which is also easy to cause bioinfestation of finished products and affect the durability of finished products

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for preparing bio-based composite material by using palm biomass powder as raw material
  • Method for preparing bio-based composite material by using palm biomass powder as raw material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Step 1. Cleaning of palm micropowder:

[0021] Generally speaking, biomass micropowder is a relatively cheap resin filler. The cost of biomass micropowder is only 300-800 yuan / ton, and the cleaning cost of biomass micropowder is even much higher than the cost of biomass micropowder itself. Because of this, practitioners in the bio-based materials industry usually do not clean and purify biomass powder. However, there are many unfavorable factors to directly use palm micropowder as biomass filling material. The content of protein and oil in palm micropowder is too high, which is easy to cause discoloration, coking, migration of small molecular substances and biological erosion, which seriously affects the production of bio-based resin. Product performance. The inventor believes that there are serious misunderstandings about the cleaning and surface treatment of biomass in the current industry. It is generally believed in the industry that water should be used as the med...

Embodiment 2

[0036] Step 1. Surface cleaning of palm micropowder:

[0037] Put 100 parts of 600-mesh palm micropowder into the reaction vessel, add 500 parts of acetone into the reaction vessel according to the bath ratio of 1:5, close the reaction vessel to seal the system, heat to 50°C, stir and disperse at a speed of 500 rpm for 30 minutes, Stand still to make the palm micropowder settle, use the press plate to slightly compact the settled solid, draw out the clear liquid above the press plate, recover the clear liquid, distill and recover a large amount of acetone solvent, and filter the remaining turbid solution, then concentrate the distillation to recover the solvent. Lift the pressure plate, add 500 parts of acetone preheated to 50°C to the reaction vessel as a dispersion medium, stir and disperse at a speed of 500 rpm for 15 minutes, let the palm fine powder settle, use the pressure plate to slightly press the settled solid Solid, pump out the clarified liquid above the platen. A...

Embodiment 3

[0043] Step 1. Surface cleaning of palm micropowder:

[0044] Put 100 parts of 800-mesh palm skin micropowder into the reaction vessel, add 400 parts of acetone into the reaction vessel according to the bath ratio of 1:4, close the reaction vessel to seal the system, heat to 60°C, stir and disperse at a speed of 500 rpm for 30 minutes , let the palm powder settle, use the press plate to slightly compact the settled solid, draw out the clear liquid above the press plate, recover the clear liquid, distill and recover a large amount of acetone solvent, filter the remaining turbid solution, and concentrate the distillation to recover the solvent. Lift the pressure plate, add 500 parts of acetone preheated to 50°C to the reaction vessel as a dispersion medium, stir and disperse at a speed of 500 rpm for 15 minutes, let the palm fine powder settle, use the pressure plate to slightly press the settled solid Solid, pump out the clarified liquid above the platen. After repeating this ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Tensile strengthaaaaaaaaaa
Particle sizeaaaaaaaaaa
Particle sizeaaaaaaaaaa
Login to View More

Abstract

The invention provides a method for preparing a bio-based composite material by using palm biomass powder as a raw material, and belongs to the technical field of preparation methods of bio-based composite materials. The method comprises the following steps: 1, cleaning palm micro-powder: putting 100 parts of 600-1200-mesh palm micro-powder into a reaction container, and adding 400-500 parts of acetone into the reaction container according to a bath ratio of 1:4 or 1:5; 2, carrying out surface treatment on the palm micro-powder: heating a reaction system subjected to solvent replacement to 80-100 DEG C, removing water from the obtained distillate by using a 3A molecular sieve, and refluxing the distillate into a reaction kettle; and 3, blending and extruding the bio-based resin. The methodsolves the problems of impurity migration and insufficient product performances, caused by too high content of oily small molecules when palm is used as the biomass raw material, breaks through the recognition misunderstanding that the biomass can only be treated in an aqueous solution and otherwise the processing cost is too high, and creates an effective palm biomass treatment method. Palm residues are used as the bio-based raw material to prepare the novel bio-based resin material having the advantages of low cost, high performances and good processability and meeting food contact conditions.

Description

technical field [0001] The invention relates to a preparation method of a bio-based composite material using palm biomass powder as a raw material, and belongs to the technical field of bio-based composite material preparation methods. Background technique [0002] Petroleum-based resins, such as general-purpose resins such as polyethylene, polypropylene, polystyrene, and polyvinyl chloride, are still indispensable, mass-produced and used in current production and life, and there is no important raw material to replace products in the short term . Since there is no substitute, reducing the use of petroleum-based resins is still one of the important development directions of the resin industry in the next few decades. The preparation of a series of resin products such as highly filled resins, bio-based resins, and bio-based composite materials is the main research content of this direction. [0003] Palm is one of the main economic crops in the tropics and subtropics. The p...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C08L97/02C08L91/00C08L23/08C08L23/12C08L67/04C08L29/04C08K3/26C08K5/098
CPCC08L97/02C08K2003/265C08K2201/014C08K2201/005C08L2205/035C08L2205/03C08L91/00C08L23/0815C08K3/26C08K5/098C08L23/12C08L67/04C08L29/04B29B7/7461B29B7/002B29B7/10B29B7/826B29B9/06B29B9/14B29B7/92B29B7/48B29B7/726B29C48/92B29C48/04B29C48/022C08G18/73C08G18/6492C08G18/7621B01D21/0039B01D21/28B29B7/005B29B9/10B29B2009/125C08L23/06C08L2207/066
Inventor 范大鹏齐海群王育钦冯钢
Owner LIAONING XINGFUREN TECH CO LTD