Application of ultraviolet rays to degradation of pyridaben residues in oolong tea
A technology of ultraviolet light and oolong tea, which is applied in tea treatment before extraction, etc., can solve the problem of excessive pyridaben pesticide residues, achieve the effect of reducing the residual content of pyridaben, ensuring food safety, and achieving sterilization
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Embodiment 1
[0013] Embodiment one: reduce the processing method of pyridaben content in oolong tea, comprise the following steps:
[0014] 1. Weigh the standard product of pyridaben, dissolve it in toluene to obtain the standard solution of pyridaben, and the concentration range is 0.1mg / kg-1000.0mg / kg.
[0015] 2. Mix the standard solution of pyridaben with oolong tea, so that the content of pyridaben in the spiked sample of oolong tea is 5.00 mg / kg.
[0016] 3. Apply the degradation method to the oolong tea spiked sample: set the wavelength of ultraviolet light (240-260nm), the time is 60min, start the ultraviolet irradiation device, and start the ultraviolet irradiation to process the oolong tea spiked sample; after the ultraviolet irradiation is finished, take out the treated oolong tea sample.
[0017] 4. Detection and extraction method of pyridaben content in oolong tea samples: Accurately weigh 5.00g of oolong tea samples, add 15mL of acetonitrile, extract homogeneously at 15000r / ...
Embodiment 2
[0037] Embodiment two: reduce the processing method of pyridaben content in oolong tea, comprise the following steps:
[0038] 1. Weigh the standard product of pyridaben, dissolve it in toluene to obtain the standard solution of pyridaben, and the concentration range is 0.1mg / kg-1000.0mg / kg.
[0039] 2. Mix the standard solution of pyridaben with oolong tea, so that the content of pyridaben in the spiked sample of oolong tea is 5.00 mg / kg.
[0040] 3. Apply the degradation method to the oolong tea spiked sample: set the wavelength of ultraviolet light (240-260nm) for 120 minutes, start the ultraviolet irradiation device, and start the ultraviolet irradiation treatment; after the ultraviolet irradiation is completed, take out the processed oolong tea sample.
[0041] 4. Detection and extraction method of pyridaben content in oolong tea samples: Accurately weigh 5.00g of oolong tea samples, add 15mL of acetonitrile, extract homogeneously at 15000r / min for 1min, centrifuge at 4200r...
Embodiment 3
[0061] Embodiment three: reduce the processing method of pyridaben content in oolong tea, comprise the following steps:
[0062] 1. Weigh the standard product of pyridaben, dissolve it in toluene to obtain the standard solution of pyridaben, the concentration range is 0.1mg / kg-1000.0mg / kg;
[0063] 2. Mix the pyridaben standard solution with oolong tea, so that the content of pyridaben in the oolong tea spiked sample is 5.00 mg / kg;
[0064] 3. Apply the degradation method to the oolong tea spiked sample: set the wavelength of ultraviolet light (240-260nm), the time is 60min, start the ultraviolet irradiation device, and start the ultraviolet irradiation to process the oolong tea spiked sample; after the ultraviolet irradiation is finished, take out the treated oolong tea sample;
[0065] 4. Detection and extraction method of pyridaben content in oolong tea samples: Accurately weigh 5.00g of oolong tea samples, add 15mL of acetonitrile, extract homogeneously at 15000r / min for ...
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