Extraction method of alpinia galanga rhizome flavonoids

A technology of galangalone and an extraction method, which is applied in the field of extraction of galangaloid compounds, can solve the problems of waste of resources, less flavonoids, low extraction yield and purity of flavonoids, etc., and achieves the effects of reducing waste and improving extraction rate.

Inactive Publication Date: 2020-03-27
防城港市绿华源农林科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] However, at present, there are very few documents about extracting flavonoids from galangal, and the extraction yield and purity of flavonoids are relatively low, which makes the active ingredients in galangal lost, resulting in waste of resources

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] A method for extracting galangal flavonoids, comprising galangal pretreatment, microwave extraction, enzymatic treatment, supercritical CO 2 The steps of extraction, vacuum concentration, and vacuum freeze-drying to obtain the turmeric ketones compound specifically include the following steps:

[0032] (1) Ginger pretreatment: remove impurities from fresh galangal, clean it, put it into a grinder with purified water and grind it to obtain galangal juice; the mass ratio of galangal to purified water is 1:1.5 ; The grinding is to grind Galangal to cross 80 mesh sieves;

[0033] (2) Microwave extraction: microwave extraction is carried out to the southern ginger juice obtained in step (1), repeat microwave extraction 3 times, obtain extract; The frequency of described microwave extraction is 0.1KHz, power is 400W, and stirring speed is 20r / min, the time is 25min;

[0034](3) Enzymolysis treatment: under agitation, add cellulase, protease and ligninase to the extract obt...

Embodiment 2

[0038] A method for extracting galangal flavonoids, comprising galangal pretreatment, microwave extraction, enzymatic treatment, supercritical CO 2 The steps of extraction, vacuum concentration, and vacuum freeze-drying to obtain the turmeric ketones compound specifically include the following steps:

[0039] (1) Ginger pretreatment: remove impurities from fresh galangal, clean it, put it into a grinder with purified water for grinding, and obtain galangal juice; the mass ratio of galangal to purified water=1:2 ; The grinding is to grind Galangal to cross 100 mesh sieves;

[0040] (2) Microwave extraction: microwave extraction is carried out to the southern ginger pulp juice that step (1) obtains, repeat microwave extraction 3 times, obtain extract; The frequency of described microwave extraction is 0.2KHz, and power is 450W, and stirring speed is 25r / min, the time is 30min;

[0041] (3) Enzymolysis treatment: under agitation, add cellulase, protease and ligninase to the ex...

Embodiment 3

[0045] A method for extracting galangal flavonoids, comprising galangal pretreatment, microwave extraction, enzymatic treatment, supercritical CO 2 The steps of extraction, vacuum concentration, and vacuum freeze-drying to obtain the turmeric ketones compound specifically include the following steps:

[0046] (1) Ginger pretreatment: remove impurities from fresh galangal, clean it, put it into a grinder with purified water and grind it to obtain galangal juice; the mass ratio of galangal to purified water is 1:1.6 ; The grinding is to grind Galangal to cross 85 mesh sieves;

[0047] (2) Microwave extraction: microwave extraction is carried out to the southern ginger pulp juice that step (1) obtains, repeat microwave extraction 3 times, obtain extract; The frequency of described microwave extraction is 0.12KHz, and power is 410W, and stirring speed is 21r / min, the time is 26min;

[0048] (3) Enzymolysis treatment: under agitation, add cellulase, protease and ligninase to the...

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PUM

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Abstract

The invention discloses an extraction method of alpinia galanga rhizome flavonoids. The extraction method of the alpinia galanga rhizome flavonoids includes the steps of: alpinia galanga rhizome preprocessing, microwave extraction, enzymolysis treatment, supercritical CO2 extraction, vacuum concentration, and vacuum freeze-drying; and by adopting the extraction method, the alpinia galanga rhizomeflavonoids are obtained. According to the extraction method of the alpinia galanga rhizome flavonoids, ways of microwaves, enzymolysis and supercritical CO2 extraction are creatively adopted to extract the alpinia galanga rhizome flavonoids, after microwave treatment, enzymolysis is carried out, therefore, the flavonoids are better dissolved out, the extraction rate of the flavonoids is increased,and waste of resources is reduced; and after supercritical CO2 extraction, no organic solvent residues exist, therefore, products are ensured to be 100% pure natural, and the flavonoids with high purity are obtained.

Description

technical field [0001] The invention belongs to the technical field of plant extraction, and in particular relates to a method for extracting galangal flavonoids. Background technique [0002] Southern ginger (Alpiniagalanga (Linn.) Willd.), also known as reed ginger, red cardamom, and galanga, is a plant of the Zingiberaceae family, a perennial herb of the Zingiberaceae family, widely distributed in tropical Asia. In Chaozhou cuisine, galangal is an essential ingredient in brine bowls. It can even be said that the presence or absence of galangal is the main difference between Chaozhou brine and brine from other places. The fruits and rhizomes of galangal are used for medicinal purposes. In recent years, studies have found that the rhizomes contain a variety of aromatic oils, flavonoids, minerals, sugars and other substances, which have multiple properties such as stimulating, activating and anti-free radicals for the skin. [0003] Meridian distribution of nature and flavo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/9062A61K125/00
CPCA61K36/9062A61K2236/19A61K2236/331A61K2236/37A61K2236/39A61K2236/51
Inventor 陈明江
Owner 防城港市绿华源农林科技有限公司
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