Laser 3D printing method for in-situ synthesized alumina particle reinforced nickel base composite

A kind of aluminum oxide particles, 3D printing technology, applied in the direction of additive processing, process efficiency improvement, additive manufacturing, etc., can solve the problems of poor distribution uniformity, poor matrix interface bonding, coarse particles, etc., to achieve good interface bonding, fine particles good, evenly distributed effect

Active Publication Date: 2020-04-10
HUNAN UNIV
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  • Application Information

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Problems solved by technology

However, the use of this technology to introduce oxide particles still has problems such as poor distribution u

Method used

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  • Laser 3D printing method for in-situ synthesized alumina particle reinforced nickel base composite
  • Laser 3D printing method for in-situ synthesized alumina particle reinforced nickel base composite

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Embodiment 1

[0020] A laser 3D printing method for in-situ synthesis of alumina particles reinforced nickel-based composite materials, comprising the following steps:

[0021] Step 1: Mix nickel-based alloy powder with pure aluminum powder, the mass percentage of pure aluminum powder is 2%, and then mechanically ball mill for 10 hours, and screen out powder with a particle size of 50 μm to 120 μm after ball milling;

[0022] Step 2: Preliminary optimization of the laser 3D printing process window to obtain the following preliminary optimization parameters: laser output power of 700-1300W, defocus amount of -2.5mm, laser spot diameter of 2-3.5mm, and scanning speed of 6-15mm / s , the powder delivery rate is 12-18g / min;

[0023] Step 3: use a colorimetric pyrometer to record the temperature change curve of the molten pool during the laser 3D printing process at fixed points, extract and calculate the average peak temperature T of the temperature change curve, the intercept t of the nickel-bas...

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Abstract

A laser 3D printing method for an in-situ synthesized alumina particle reinforced nickel base composite comprises the steps that firstly, nickel base alloy and pure aluminum powder are subjected to mechanical ball milling, particle size screening is carried out on the powder obtained after ball milling, and a laser 3D printing technological window is initially optimized; a temperature changing curve of a molten pool is recorded regularly with a colorimetric pyrometer, and the average peak temperature T of the temperature curve, the intercept t of the solid phase line and the temperature curveand the average cooling rate Xi of the molten pool are extracted and calculated; and technological parameters are optimized according to the principles that T is higher than or equal to 1.4 Tm and lower than or equal to 1.8 Tm, t is larger or equal to 0.55 s and smaller than or equal to 0.95 s and Xi is larger than or equal to 3.5*103 DEG C/s, and an optimized technological window is obtained, wherein the laser output power is 800-1200 W, the defocusing amount is -2.5 mm, the diameter of a laser spot is 2-3 mm, the scanning speed is 8-14 mm/s, and the powder feeding amount is 12-16 g/min. By means of the laser 3D printing method, in-situ synthesis of alumina particles can be achieved in the forming process, and the mechanical performance of nickel base forming parts can be improved.

Description

technical field [0001] The invention relates to the field of laser material processing, in particular to a laser 3D printing method for in-situ synthesis of aluminum oxide particle-reinforced nickel-based composite materials. Background technique [0002] Nickel-based superalloys are widely used in aviation, aerospace and energy fields due to their good high-temperature mechanical properties and corrosion resistance, such as the manufacture of key components of steam turbines and aero-engines. Because the working environment of nickel-based superalloys is usually very harsh, such as high temperature, high pressure and oxidation corrosion, etc., and with the rapid development of aviation, aerospace engine and gas turbine technology, the applicable temperature and high-temperature performance of nickel-based superalloy materials are higher. requirements. Generally, directionally solidified crystals and single crystals can effectively improve the high-temperature performance o...

Claims

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Application Information

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IPC IPC(8): B22F1/00B22F9/04B22F3/105C22C19/03B33Y10/00B33Y50/02B33Y70/00
CPCB22F9/04C22C19/03B33Y10/00B33Y50/02B33Y70/00B22F2009/043B22F10/00B22F1/05B22F10/368B22F10/36Y02P10/25
Inventor 肖辉谢盼宋立军易黄懿肖文甲成满平罗国云
Owner HUNAN UNIV
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