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Upflow reactor and its application

A reactor and upflow technology, applied in chemical instruments and methods, hydrocarbon oil treatment, chemical/physical processes, etc., can solve problems such as uneven distribution of fluid gas, influence on fluid distribution, blockage of distributors, etc., to ensure long cycle Operation, ensuring the effect of use, and reducing the effect of dust generation

Active Publication Date: 2021-10-08
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since the catalyst particles cannot pass through the small bed support gap, these particles are likely to block the distributor or bed support, resulting in uneven distribution of fluid, especially gas, which affects the distribution of fluid in the reactor and affects the reaction process. adversely affect
At the same time, it will also be accompanied by the wear and pulverization of the catalyst particles, resulting in a large amount of catalyst dust. These dusts move upward with the reaction materials, and clogging occurs on the surface of the screen or grid, resulting in a rapid increase in the pressure drop of the bed, affecting response start cycle

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049]Using the upflow reactor described in the present invention, the raw material oil and hydrogen are mixed using a conventional static mixer (model SX2.3 / 20-6.4-500), and then the mixture is introduced into the present invention as a reactor feed The upflow reactor (reactor diameter is 100mm), the reactor is filled with catalyst support grid, protective agent layer 100mm, first catalyst bed layer 550mm, first floating grid and dust removal combination layer in sequence along the material flow direction 200mm; the catalyst bed supporting grid is slatted, and a 10-mesh screen is laid flat on the surface of the grid. The first floating grille and dust removal combination layer includes floating grille interlayer, separation unit and slideway. The floating grille interlayer is movably connected on the slideway, and the length of the slideway is 200mm; the grille interlayer includes upper grille plate, lower grille The fixed interlayer between the grid plate, the upper grid pla...

Embodiment 2

[0051] Using the upflow reactor of the present invention, the raw material oil and hydrogen are mixed with an inorganic membrane tube disperser. First, the hydrogen is dispersed into microbubbles with a size of 50nm and then penetrates out of the tube to form a reaction with the liquid introduced into the shell. The mixture is fed to the reactor, and then the mixture is introduced into the upflow reactor of the present invention as the reactor feed (the diameter of the upflow reactor is DN200×1000mm); the upflow reactor is sequentially filled with support grids, The protective agent layer is 100mm, the first catalyst bed is 300mm, the first floating grid and dedusting combination layer is 120mm, the second catalyst bed is 400mm, the second floating grid and dedusting combined layer is 80mm; catalyst bed supporting grid Grid, 10-mesh screen spread on the surface of the grid plate. The first floating grille and dust removal combination layer includes a floating grille interlayer...

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Abstract

The invention discloses an up-flow reactor and its application. The up-flow reactor comprises a reactor shell, and a support grid, a catalyst bed, a floating grid and a dust removal combination are arranged in the reactor shell along the material flow direction. The bottom of the reactor shell is provided with a reaction material inlet, and the top of the reactor shell is provided with a reaction material outlet. The floating grid and the dust removal combined layer are arranged in the reactor, which can effectively reduce the movement and wear between the catalyst particles, improve the service life of the catalyst, continuously remove the catalyst dust during the reaction process, improve the reaction uniformity, and greatly reduce the speed of the reaction. The pressure drop of the catalyst bed is increased to maintain the long-term stable operation of the reactor.

Description

technical field [0001] The invention belongs to the field of petrochemical equipment, and relates to an upflow reactor and its application. Background technique [0002] In the field of petrochemical industry, hydrogenation process is an important technical means for processing distillate oil and secondary processed oil. Through hydrogenation, impurities such as sulfur, nitrogen, metals, colloids, and residual carbon in oil products can be effectively removed. Removal and hydrogenation of unsaturated hydrocarbons to saturated hydrocarbons. According to the type of reactor, the hydrogenation process can be divided into fixed bed hydrogenation process, suspension bed hydrogenation process and ebullated bed hydrogenation process, among which the fixed bed hydrogenation process is the most widely used. [0003] According to the feeding method of the fixed bed reactor, it can be divided into two types: upflow type, that is, bottom feed and downflow type, that is, top feed fixed ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/04C10G49/00
CPCB01J8/0446B01J8/0492B01J2208/00884C10G49/00C10G2300/4006C10G2300/4012
Inventor 杨秀娜阮宗琳王昊晨姜阳崔国英周嘉文关明华
Owner CHINA PETROLEUM & CHEM CORP
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