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Camellia extract as well as preparation method and application thereof, and cosmetic containing camellia extract

A technology of camellia flower and extract is applied in the field of camellia flower extract, its preparation method and application, and the field of cosmetics containing the same, which can solve the problems of low extraction rate, low activity of the extract, low content of active ingredients in the extract, etc., and achieves anti-oxidation Strong activity, good for skin absorption

Pending Publication Date: 2020-07-14
GUANGDONG MARUBI BIOLOGICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the existing above-mentioned extraction process generally has the problems of low extraction rate, low content of active ingredients in the obtained extract and low activity of the extract.

Method used

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  • Camellia extract as well as preparation method and application thereof, and cosmetic containing camellia extract
  • Camellia extract as well as preparation method and application thereof, and cosmetic containing camellia extract
  • Camellia extract as well as preparation method and application thereof, and cosmetic containing camellia extract

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preparation example Construction

[0049] According to one aspect of the present invention, a kind of preparation method of camellia extract, described preparation method comprises the following steps:

[0050] Ultrasonic extraction of camellia, and then reacting the extract with a metal ion complexing agent to obtain a precipitate A; then sequentially trans-solubilizing and extracting the precipitate A to obtain a camellia extract;

[0051] The ultrasonic extraction solvent includes ethanol and ammonium sulfate.

[0052]The preparation method of the camellia extract provided by the present invention, the preparation method first ultrasonically extracts the camellia, and then reacts the extract with a metal ion complexing agent to obtain a precipitate A; then the precipitate A is sequentially transferred and extracted, Camellia flower extract is obtained; the ultrasonic extraction solvent includes ethanol and ammonium sulfate. The above-mentioned preparation method first uses ethanol and ammonium sulfate as ul...

Embodiment 1

[0107] A kind of preparation method of camellia extract, described preparation method comprises the following steps:

[0108] (1) Crush the camellia into a 20-mesh sieve powder, add the extraction solvent according to the ratio of material to liquid of 1:30, and extract with ultrasound for 20 minutes under the conditions of ultrasonic power of 75kHZ and extraction temperature of 25°C, and then centrifuge at 4400rmp for 10min , extract the upper ethanol phase solution to obtain the extract;

[0109] In percent by volume, the extraction solvent includes 40% of absolute ethanol and 60% of ammonium sulfate aqueous solution;

[0110] The concentration of the ammonium sulfate aqueous solution is 0.28g / L;

[0111] (2), the content of tea polyphenols in the extract obtained in step (1) was detected by Folin’s phenol method to 4.003mg / mL, then aluminum chloride was added to the extract and mixed evenly and allowed to stand for 15min, then the extract Centrifuge at 4400rmp for 10min t...

Embodiment 2

[0117] A kind of preparation method of camellia extract, described preparation method comprises the following steps:

[0118] (1) Crush the camellia into a powder passing through a 200-mesh sieve, add an extraction solvent at a material-to-liquid ratio of 1:30, and conduct ultrasonic extraction for 30 minutes at an ultrasonic power of 80kHZ and an extraction temperature of 35°C, followed by centrifugation at 4400rmp for 10 minutes , extract the upper ethanol phase solution to obtain the extract;

[0119] In percent by volume, the extraction solvent includes 50% absolute ethanol and 50% ammonium sulfate aqueous solution;

[0120] The concentration of the ammonium sulfate aqueous solution is 0.32g / L;

[0121] (2), Utilize the tea polyphenols content in the extract obtained in step (1) to detect by Folin’s phenol method, then add the metal ion complexing agent into the extract and mix well and let it stand for 15min, then centrifuge the extract at 4400rmp 10min, obtain precipit...

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Abstract

The invention provides a camellia extract as well as a preparation method and an application thereof, and a cosmetic containing the camellia extract, and relates to the technical field of deep processing of camellia products. The preparation method comprises the following steps of firstly, performing ultrasonic extraction on camellia, and then performing a reaction between an extracting solution and a metal ion complexing agent to obtain a precipitate A; and sequentially carrying out decreaming and extraction on the precipitate A to obtain a camellia extract, wherein the ultrasonic extractionsolvent comprises ethanol and ammonium sulfate. The camellia extract extracted by the preparation method has the advantages of high extraction rate and strong antioxidant activity; and meanwhile, thepreparation method is mild in condition and easy to operate, and is very suitable for industrial large-scale production.

Description

technical field [0001] The invention relates to the technical field of deep processing of camellia products, in particular to a camellia extract, its preparation method and application, and cosmetics containing the same. Background technique [0002] Camellia is a general term for various plants of the family Theaceae and the genus Camellia. Camellia is prized by the world's horticultural circles for its beautiful plant shape and colorful flower shapes. Camellia is also widely planted in China's Yangtze River Basin, Pearl River Basin, Chongqing, Yunnan, and Sichuan, as well as in North Korea, Japan, and India. It is one of the world's rare flowers and trees. Existing studies have shown that the flowers, leaves and buds of camellia are rich in various amino acids, vitamins and various trace elements, which can be easily absorbed by the skin, provide skin care nutrients, and effectively lock in the moisture of the surface cells of the skin , restore moisture and vitality to ...

Claims

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Application Information

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IPC IPC(8): A61K8/9789A61Q19/08
CPCA61K8/9789A61Q19/08A61K2800/82A61K2800/84A61K2800/805
Inventor 裴运林聂艳峰杨盼盼郭朝万王娟蒲艳
Owner GUANGDONG MARUBI BIOLOGICAL TECH CO LTD
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