Agilawood fire-free aromatherapy liquid as well as preparation method and application thereof
A kind of technology of agarwood and fire incense, which is applied in the field of agarwood fire-free aromatherapy liquid and its preparation, which can solve the problems of different fragrance types, insufficient fragrance, hidden dangers of electricity safety, etc., and achieve the effect of pure fragrance
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Embodiment 1
[0038] A kind of agarwood pure dew, obtained by the following preparation method:
[0039] (1) Pretreatment: select the raw material of agarwood, pulverize the agarwood, and pass through a 40-mesh sieve to obtain agarwood granules.
[0040] (2) Extraction: place the agarwood granules in supercritical CO 2 In the equipment, set the system pressure to 28MPa, the system flow rate to 210L / min, the extraction temperature to 60°C, and the extraction time to 120min to obtain the Agarwood extract.
[0041] (3) Molecular cutting: Use the MDS-80 molecular cutting machine to precisely cut the incense segment of the above-mentioned agarwood paste extract. 200r / min, the cutting temperature of column 1 is 100°C, the cutting temperature of column 2 is 135°C, the collection temperature of column 1 is 35°C, the collection temperature of column 2 is 15°C, discard the first and last section products, and keep the middle section products, The product in the middle section is agarwood essential ...
Embodiment 2
[0044] A kind of agarwood pure dew, obtained by the following preparation method:
[0045] (1) Pretreatment: select the raw material of agarwood, pulverize the agarwood, and pass through a 50-mesh sieve to obtain agarwood granules.
[0046] (2) Extraction: place the agarwood granules in supercritical CO 2 In the equipment, set the system pressure to 25MPa, the system flow rate to 210L / min, the extraction temperature to 55°C, and the extraction time to 120min to obtain agarwood paste extract.
[0047] (3) Molecular cutting: use the MDS-80 molecular cutting machine to precisely cut the above-mentioned agarwood paste extract, the cutting vacuum is 1Pa, the speed of the scraping film of column 1 is 210r / min, and the speed of scraping film of column 2 is 210r / min, the cutting temperature of column 1 is 90°C, the cutting temperature of column 2 is 120°C, the collection temperature of column 1 is 30°C, and the collection temperature of column 2 is 12°C. The segment product is agar...
Embodiment 3
[0050] A kind of agarwood pure dew, obtained by the following preparation method:
[0051] (1) Pretreatment: select the raw material of agarwood, pulverize the agarwood, and pass through a 60-mesh sieve to obtain agarwood granules.
[0052] (2) Extraction: place the agarwood granules in supercritical CO 2 In the equipment, set the system pressure to 30MPa, the system flow rate to 210L / min, the extraction temperature to 65°C, and the extraction time to 120min to obtain agarwood paste extract.
[0053] (3) Molecular cutting: Use the MDS-80 molecular cutting machine to precisely cut the incense segment of the above-mentioned agarwood paste extract, the cutting vacuum is 10Pa, the speed of the scraping film of column 1 is 230r / min, and the speed of scraping film of column 2 is 230r / min, the cutting temperature of column 1 is 100°C, the cutting temperature of column 2 is 140°C, the collection temperature of column 1 is 40°C, and the collection temperature of column 2 is 20°C. Th...
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