Agilawood fire-free aromatherapy liquid as well as preparation method and application thereof
A kind of technology of agarwood and fire incense, which is applied in the field of agarwood fire-free aromatherapy liquid and its preparation, which can solve the problems of different fragrance types, insufficient fragrance, hidden dangers of electricity safety, etc., and achieve the effect of pure fragrance
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[0037] Example 1
[0038] A kind of agarwood pure lotion, obtained by the following preparation method:
[0039] (1) Pretreatment: select agarwood raw materials, pulverize agarwood, and pass a 40-mesh sieve to obtain agarwood particles.
[0040] (2) Extraction: Place agarwood particles in supercritical CO 2 In the equipment, the system pressure is set to 28MPa, the system flow rate is 210L / min, the extraction temperature is 60°C, and the extraction time is 120min to obtain agarwood extract.
[0041] (3) Molecular cutting: Use MDS-80 molecular cutting machine to accurately cut the incense segment of the above-mentioned agarwood paste extract. The cutting vacuum is 0.1Pa, the scraping speed of column 1 is 200r / min, and the scraping speed of column 2 is 200r / min, column 1 cutting temperature is 100°C, column 2 cutting temperature is 135°C, column 1 collection temperature is 35°C, column 2 collection temperature is 15°C, discard the first and last products, and keep the intermediate produ...
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[0043] Example 2
[0044] A kind of agarwood pure lotion, obtained by the following preparation method:
[0045] (1) Pretreatment: select agarwood raw materials, pulverize agarwood, and pass a 50-mesh sieve to obtain agarwood particles.
[0046] (2) Extraction: Place agarwood particles in supercritical CO 2 In the equipment, the system pressure is set to 25MPa, the system flow rate is 210L / min, the extraction temperature is 55°C, and the extraction time is 120min to obtain agarwood paste extract.
[0047] (3) Molecular cutting: use MDS-80 molecular cutting machine to accurately cut the incense segment of the above-mentioned agarwood paste extract, the cutting vacuum is 1Pa, the scraping speed of column 1 is 210r / min, and the scraping speed of column 2 is 210r / min, the cutting temperature of column 1 is 90°C, the cutting temperature of column 2 is 120°C, the collection temperature of column 1 is 30°C, and the collection temperature of column 2 is 12°C. The first and last products are ...
Example Embodiment
[0049] Example 3
[0050] A kind of agarwood pure lotion, obtained by the following preparation method:
[0051] (1) Pretreatment: select agarwood raw materials, pulverize agarwood, and pass a 60-mesh sieve to obtain agarwood particles.
[0052] (2) Extraction: Place agarwood particles in supercritical CO 2 In the equipment, the system pressure is set to 30MPa, the system flow rate is 210L / min, the extraction temperature is 65°C, and the extraction time is 120min to obtain agarwood paste extract.
[0053] (3) Molecular cutting: use MDS-80 molecular cutting machine to accurately cut the incense segment of the above-mentioned agarwood paste extract. The cutting vacuum is 10Pa, the scraping speed of column 1 is 230r / min, and the scraping speed of column 2 is 230r. / min, column 1 cutting temperature is 100℃, column 2 cutting temperature is 140℃, column 1 collection temperature is 40℃, column 2 collection temperature is 20℃, discard the first and last products, keep the intermediate produc...
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