High-adhesion water transfer printing water-based paint and preparation method thereof
A water-based paint, high adhesion technology, applied in the field of paint, to achieve the effect of easy paint removal, good adhesion and construction
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Embodiment 1
[0033] A preparation method for high adhesion water transfer printing water-based paint, comprising the following steps
[0034] (1) Preparation of modified aqueous acrylic resin dispersion:
[0035] (1-1) Add a certain amount of isopropanol to a 250ml four-necked flask equipped with a reflux condenser, a constant pressure dropping funnel, a mechanical stirrer, and a thermometer, and stir until the reflux temperature (about 82°C) is reached, and wait until the reflux is stable Afterwards, the monomer mixture of MMA, BA, AA, HEMA, and AIBN was added dropwise within 40-60 minutes. 20min after the dropwise addition,
[0036] (1-2) Start to add HEA and a small amount of AIBN dropwise, and the dropwise addition is completed in about 15 minutes; then raise the temperature to 85°C, and keep the temperature for 3 hours.
[0037] (1-3) Then, cool down to 50°C and add ammonia water to adjust the pH of the system to 7-8, add deionized water after about 10 minutes and stir vigorously. ...
Embodiment 2
[0049] A preparation method for high adhesion water transfer printing water-based paint, comprising the following steps
[0050] (1) Preparation of modified aqueous acrylic resin dispersion:
[0051] (1-1) Add a certain amount of isopropanol to a 250ml four-necked flask equipped with a reflux condenser, a constant pressure dropping funnel, a mechanical stirrer, and a thermometer, and stir until the reflux temperature (about 82°C) is reached, and wait until the reflux is stable Afterwards, the monomer mixture of MMA, BA, AA, HEMA and AIBN was added dropwise within 40-60 minutes.
[0052] (1-2) 20 minutes after the dropwise addition, start to add HEA and a small amount of AIBN dropwise, and the dropwise addition is completed in about 15 minutes; then raise the temperature to 85°C, and keep the temperature for 3 hours.
[0053] (1-3) Then, cool down to 50°C and add ammonia water to adjust the pH of the system to 7-8, add deionized water after about 10 minutes and stir vigorously...
Embodiment 3
[0064] A preparation method for high adhesion water transfer printing water-based paint, comprising the following steps
[0065] (1) Preparation of modified aqueous acrylic resin dispersion:
[0066] (1-1) Add a certain amount of isopropanol to a 250ml four-necked flask equipped with a reflux condenser, a constant pressure dropping funnel, a mechanical stirrer, and a thermometer, and stir until the reflux temperature (about 82°C) is reached, and wait until the reflux is stable Afterwards, the monomer mixture of MMA, BA, AA, HEMA and AIBN was added dropwise within 40-60 minutes.
[0067] (1-2) 20 minutes after the dropwise addition, start to add HEA, MMA (1:1) and a small amount of AIBN dropwise, and the dropwise addition is completed in about 15 minutes; then raise the temperature to 85°C, and keep the temperature for 3 hours.
[0068] (1-3) Then, cool down to 50°C and add ammonia water to adjust the pH of the system to 7-8, add deionized water after about 10 minutes and stir...
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