Manufacturing method of R-T-B series sintered magnet
A technology of sintered magnets and manufacturing methods, which can be applied in the manufacture of inductors/transformers/magnets, magnetic objects, and manufacture of motor generators, etc., and can solve problems such as easy demagnetization
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[0112] Each element was weighed so that the RTB-based sintered magnets had approximately the compositions shown in alloy Nos. M1 to M6 in Table 1, and cast by a strip casting method to obtain flaky alloys. The obtained flaky alloy was subjected to hydrogen embrittlement in a pressurized hydrogen atmosphere, and then subjected to a dehydrogenation treatment in which it was heated to 550° C. in a vacuum and then cooled to obtain a coarsely pulverized powder. Next, 0.04% by mass of zinc stearate was added as a lubricant to 100% by mass of the coarsely pulverized powder as a lubricant, and after mixing, it was mixed with a jet mill (jet mill) in a nitrogen atmosphere. Dry pulverization in the atmosphere to obtain D 50 3.8 ~ 4.0μm alloy powder. The results of component analysis of the obtained alloy powders are shown in Alloy Nos. M1 to M6 in Table 1. Each component (except O, N, and C) in Table 1 was measured by high-frequency inductively coupled plasma optical emission spectrom...
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