Ion exchange membrane and energy storage device comprising same
An ion exchange membrane, energy storage device technology, applied in electrochemical generators, fuel cells, regenerative fuel cells, etc., can solve the problems of complex synthesis methods, difficult mass production, and reduced ion exchange membrane efficiency, and prevent deterioration. , the effect of preventing ion penetration and improving voltage efficiency
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manufacture Embodiment 1
[0224] [Manufacturing Example 1: Manufacture of Ion Conductor]
manufacture Embodiment 1-1
[0226] 1) Making hydrophobic repeating units
[0227] As shown in Scheme 3 below, in the presence of potassium carbonate, bisphenol A and 1,3-bis(4-fluorobenzoyl)benzene were reacted at 160°C to 180°C for 30 hours, drained into purified water for washing, and dried using hot air. At this time, in order to adjust the degree of polymerization of the oligomer, Carother's equation was used.
[0228] [reaction formula 3]
[0229]
[0230] 2) Manufacture of hydrophilic repeating units
[0231] As shown in Equation 4 below, in the presence of potassium carbonate, 4,4'-(9-fluorenylene)bisphenol and bis(4-fluorophenyl)sulfone were prepared at 160°C using a co-solvent of DMAc / toluene It was reacted at 180° C. for 30 hours, discharged into purified water for washing, and dried using hot air. At this time, in order to adjust the degree of polymerization of the oligomer, Carother's equation was used.
[0232] [Reaction 4]
[0233]
[0234] 3) Manufacture of polymers
[0...
manufacture Embodiment 1-2
[0239] An ion conductor was produced in the same manner as in Production Example 1-1 except that, unlike Production Example 1-1, a polymer was produced such that the molar ratio of the hydrophilic repeating unit to the hydrophobic repeating unit was 1:2.5.
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