Anti-wear lubricant composition, preparation method thereof and trace lubricant prepared from the composition

A technology of anti-wear lubricants and micro lubricants, applied in the field of lubrication, can solve the problems of environmentally unfriendly sulfur and chlorine-containing additives, environmental impact, large amount of lubricant usage, etc., and achieve remarkable environmental protection effects and strong ductility Excellent elasticity and anti-friction properties

Pending Publication Date: 2020-11-03
SHANGHAI JINZHAO ENERGY SAVING TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The traditional metal cutting process uses mineral oil or vegetable oil or cutting fluid for a large amount of shower lubrication. The amount of lubricant used is large, which not only wastes resources, but also causes huge pollution to the processing site and the environment, and also seriously affects the health of the operators.
[0003] In order to solve these problems, some progress has been made in the research of micro-quantity lubrication technology recently. The micro-quantity lubrication technology solves the problems of large amount of lubricant used and serious pollution, but excessive use of sulfur and chlorine-containing additives that are not friendly to the environment , will have a certain impact on the environment
At the same time, when processing difficult-to-machine metals, it is often difficult to achieve the desired effect with minimal lubrication

Method used

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  • Anti-wear lubricant composition, preparation method thereof and trace lubricant prepared from the composition
  • Anti-wear lubricant composition, preparation method thereof and trace lubricant prepared from the composition

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Weigh 191.14 g (1 mol) of aminotriacetic acid, 716.52 g (2.4 mol) of isoeicosanol, 250 g of polyethylene glycol (PEG1000), and 20 g of phosphotungstic acid and place them in the reaction kettle, stir and heat to 180 ° C, and fully react for 5 hour, the reaction process is decompressed and drained twice, and after the reaction is completed, the water is decompressed to remove water; that is, an anti-wear lubricant composition.

[0035] The above-prepared anti-wear lubricant composition and water are mixed uniformly in a weight ratio of 1:2, and the mixture can be used in a micro-lubrication device.

Embodiment 2

[0037] Weigh aminotriacetic acid 191.14g (1mol), isooctanol 325.58g (2.5mol), polyethylene glycol (PEG200) 98g, phosphotungstic acid 10g and place in the reactor, stir and heat to 180 ℃, fully react for 6 hours , the reaction process is decompressed and drained twice, and after the reaction is completed, the water is decompressed to remove water; that is, an anti-wear lubricant composition.

[0038] Weigh 400 g of anti-wear lubricant composition, 300 g of diisooctyl 2,5-furandicarboxylate, 100 g of sodium lauroyl sarcosinate, 50 g of fatty alcohol polyoxyethylene ether (AEO-12), and 150 g of deionized water. It is a micro-lubricant when mixed at room temperature until translucent.

[0039] The preparation method of above-mentioned 2,5-furandicarboxylic acid diisooctyl ester:

[0040] 156.09g (1mol) of 2,5-furandicarboxylic acid, 286.51g (2.2mol) of isooctanol and 8g of dilute sulfuric acid (10%) were added to the reaction kettle, and the reaction was carried out at a reaction...

Embodiment 3

[0042] Weigh aminotriacetic acid 191.14g (1mol), isodecyl alcohol 316.56g (2mol), polyethylene glycol (PEG400) 150g, phosphotungstic acid 7g and place in the reactor, stir and heat to 200 ℃, fully react for 5 hours, During the reaction process, the water is decompressed and drained once, and after the reaction is completed, the water is decompressed to remove water; that is, an anti-wear lubricant composition.

[0043] Weigh 300 g of anti-wear lubricant composition, 400 g of diisodecyl 2,5-furandicarboxylate, 50 g of sodium lauroyl sarcosinate, 100 g of fatty alcohol polyoxyethylene ether (AEO-10), and 150 g of deionized water. It is a micro-lubricant when mixed and stirred at room temperature until transparent.

[0044] The preparation method of above-mentioned 2,5-furandicarboxylic acid diisodecyl ester: add 2,5-furandicarboxylic acid 156.09g (1mol), isodecyl alcohol 316.56g (2mol), 2g phosphotungstic acid in the The reaction is carried out at a reaction temperature of 180°...

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PUM

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Abstract

The invention provides an antiwear lubricant composition which is characterized by being prepared from nitrilotriacetic acid, fatty alcohol, polyethylene glycol and phosphotungstic acid, and the molarratio of nitrilotriacetic acid to fatty alcohol is 1 : 2-2.5; wherein the weight ratio of the fatty alcohol to the polyethylene glycol is 100 : 30-50; the weight of the phosphotungstic acid accountsfor 1-2% of the total weight of the nitrilotriacetic acid, the fatty alcohol and the polyethylene glycol. The anti-wear lubricant composition prepared by the invention is a PWN-containing extreme pressure anti-wear additive, has excellent anti-friction performance, and is also a good nonionic surfactant. The trace lubricant containing the anti-wear lubricant composition is prepared from the following components in percentage by weight: 30-40% of the anti-wear lubricant composition; 30-40% of 2,5-furandicarboxylic acid dialiphatic alcohol ester; 5-10% of sodium lauroyl sarcosine; 5-10% of fattyalcohol-polyoxyethylene ether; and the balance deionized water.

Description

technical field [0001] The invention belongs to the technical field of lubrication, and in particular, relates to an anti-wear lubricant composition, a preparation method thereof, and a trace lubricant prepared by the composition. Background technique [0002] The traditional metal cutting process uses mineral oil or vegetable oil or cutting fluid for a large amount of shower lubrication. The use of lubricant is large, which not only wastes resources, causes huge pollution to the processing site and the environment, but also seriously affects the health of operators. . [0003] In order to solve these problems, some progress has been made in the recent research on the minimal quantity lubrication technology. The minimal quantity lubrication technology solves the problems of the above-mentioned lubricants such as large amount of use and serious pollution, but excessive use of sulfur-containing and chlorine-containing additives that are not friendly to the environment. , will...

Claims

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Application Information

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IPC IPC(8): C10M173/02C10M161/00C10M177/00C07D307/68C10N30/06C10N30/12C10N40/22
CPCC10M173/02C10M161/00C10M177/00C07D307/68C10M2215/04C10M2209/104C10M2201/085C10M2227/066C10M2207/282C10M2215/08C10M2209/108
Inventor 张乃庆吴启东蒋宁邱秋敏
Owner SHANGHAI JINZHAO ENERGY SAVING TECH
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