Novel compound and organic light-emitting device comprising same
A compound and chemical formula technology, applied in the field of novel compounds and organic light-emitting devices containing them, can solve the problems of high driving voltage, low efficiency, short life, etc., and achieve the effect of low driving voltage, excellent arrangement, roll-off and long life
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1 to 20
[0214] Examples 1 to 20: Synthesis of Compounds
[0215] Using the above intermediates IM1 to IM11, the target compounds 1 to 20 were synthesized as follows.
Embodiment 1
[0216] Embodiment 1: the synthesis of compound 1
[0217]
[0218] In a round bottom flask, 3.0 g of IM1, 2.17 g of di([1,1'-biphenyl]-4-yl)amine (di([1,1'-biphenyl]-4-yl)amine) , 0.9g of t-BuONa, 0.2g of Pd 2 (dba) 3 , 0.3ml of (t-Bu) 3 After P was dissolved in 80 ml of toluene, stirring was performed under reflux. The reaction was confirmed by thin layer chromatography, and the reaction was terminated after adding water. The organic layer was extracted with dichloromethane, filtered under reduced pressure, followed by column purification and recrystallization to obtain 3.0 g of Compound 1 (yield 67%).
[0219] m / z: 729.27 (100.0%), 730.27 (58.9%), 731.27 (17.4%), 732.28 (3.2%)
Embodiment 2
[0220] Embodiment 2: the synthesis of compound 2
[0221]
[0222] Utilize N-([1,1'-biphenyl]-4-yl)naphthalen-1-amine (N-([1,1'-biphenyl]-4-yl)naphthalen-1-amine) to replace di( [1,1'-biphenyl]-4-yl)amine, compound 2 was synthesized in the same manner as compound 1 (yield 63%).
[0223] m / z: 703.25 (100.0%), 704.25 (56.6%), 705.26 (16.2%), 706.26 (3.1%)
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 


