Botanical hygienic insecticide and preparation method thereof
An insecticide, a plant-derived technology, which is applied to the field of plant-derived sanitary insecticides and their preparation, can solve the problems of low safety, low antibacterial activity, and low medicinal efficacy, and achieves environmental protection, enhanced bactericidal properties, and medicinal efficacy. quick effect
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Embodiment 1
[0031] A botanical hygienic insecticide is characterized in that it comprises the following components in mass percentage: modified cytisine-matrine 1%, tourmaline / allyl trimethylsiloxane / allyl 1% triphenylphosphonium bromide, 1% cocoyl glucoside, 1% saikosaponin, and the balance is water.
[0032] Further, the preparation method of the citric acid / cytisine-matrine comprises the following steps:
[0033] Step 1, preparation of cytisine-matrine: grinding cytisine and matrine into powder, and mixing uniformly to obtain cytisine-matrine;
[0034] Step II, preparation of modified cytisine-matrine: add the cytisine-matrine obtained in step I into an organic solvent, stir until dissolved and mix uniformly at 30°C, avoiding Light and nitrogen protection, then add citric acid, raise the temperature to 50°C, react for 4h, cool to room temperature, concentrate to obtain modified cytisine-matrine.
[0035] Further, the molar ratio of cytisine and matrine in the step I is 1:1.
[0036]...
Embodiment 2
[0044] A botanical hygienic insecticide is characterized in that it includes the following components in mass percentage: modified cytisine-matrine 1.3%, tourmaline / allyl trimethylsiloxane / allyl 1.5% triphenylphosphonium bromide, 1.5% cocoyl glucoside, 1.5% saikosaponin, and the balance is water.
[0045] Further, the preparation method of the citric acid / cytisine-matrine comprises the following steps:
[0046] Step 1, preparation of cytisine-matrine: grinding cytisine and matrine into powder, and mixing uniformly to obtain cytisine-matrine;
[0047] Step II, preparation of modified cytisine-matrine: add the cytisine-matrine obtained in step I into an organic solvent, stir until dissolved and mix uniformly at 35°C, avoiding Light and nitrogen protection, then add citric acid, raise the temperature to 55°C, react for 5h, cool to room temperature, concentrate to obtain modified cytisine-matrine.
[0048] Further, the molar ratio of cytisine and matrine in the step I is 1.5:1. ...
Embodiment 3
[0057] A botanical hygienic insecticide is characterized in that it includes the following components in mass percentage: modified cytisine-matrine 1.5%, tourmaline / allyl trimethylsiloxane / allyl 2% triphenylphosphonium bromide, 2% cocoyl glucoside, 2% saikosaponin, and the balance is water.
[0058] Further, the preparation method of the citric acid / cytisine-matrine comprises the following steps:
[0059] Step 1, preparation of cytisine-matrine: grinding cytisine and matrine into powder, and mixing uniformly to obtain cytisine-matrine;
[0060] Step II, preparation of modified cytisine-matrine: add the cytisine-matrine obtained in step I into an organic solvent, stir until dissolved and mix uniformly at 40°C, avoid Light and nitrogen protection, then add citric acid, raise the temperature to 60°C, react for 6h, cool to room temperature, concentrate to obtain modified cytisine-matrine.
[0061] Further, the molar ratio of cytisine and matrine in the step I is 2:1.
[0062] F...
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