Antistatic scratch-resistant tempered film
An antistatic and tempered film technology, which is applied in the direction of conductive coatings, coatings, polyurea/polyurethane coatings, etc., can solve the problems of scratch resistance of tempered films, easy dust accumulation of tempered films, loss of antistatic effect of tempered films, etc., to achieve The effect of good antistatic performance or scratch resistance performance
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Embodiment 1
[0053]An antistatic and scratch-resistant tempered film, comprising a tempered film body and a scratch-resistant and antistatic layer located on the side of the tempered film body away from the screen, wherein the preparation method of the antistatic and scratch-resistant tempered film is as follows:
[0054] (1) Preparation of starch-acrylic acid graft copolymer
[0055] S1: Add 30kg of cornstarch into 120kg of water and mix evenly, then heat up to 55°C, reflux and stir for 40min to obtain starch solution A;
[0056] S2: Add 0.05kg of initiator and 0.4kg of crosslinking agent to 40kg of methacrylic acid solution with a mass concentration of 20%, stir until dissolved and mix uniformly to obtain mixture B; wherein, potassium persulfate is used as the initiator in this embodiment , the crosslinking agent is 1,4-butanediol ester;
[0057] S3: Under the protection of nitrogen, add the mixture B to the starch solution A, then raise the temperature to 55°C, reflux and stir for 1 ho...
Embodiment 2
[0065] An antistatic and scratch-resistant tempered film differs from Example 1 in that:
[0066] (1) Preparation of starch-acrylic acid graft copolymer
[0067] S1: Add 37kg of cornstarch into 120kg of water and mix evenly, then heat up to 65°C, reflux and stir for 30min to obtain starch solution A.
[0068] S2: Add 0.1kg of initiator and 0.8kg of crosslinking agent into 50kg of methacrylic acid solution with a mass concentration of 20%, stir until dissolved and mix uniformly to obtain mixture B; wherein, ammonium persulfate is used as the initiator in this embodiment , The cross-linking agent adopts aluminum sulfate.
[0069] S3: Under the protection of nitrogen, add the mixture B to the starch solution A, then raise the temperature to 50°C, reflux and stir for 1.2h, then add 0.6kg of 1,4-hydroquinone, stir well and let it stand for 30min. A starch-acrylic acid graft copolymer was obtained.
[0070] (2) Preparation of scratch-resistant and antistatic filler
[0071] Put ...
Embodiment 3
[0073] An antistatic and scratch-resistant tempered film differs from Example 1 in that the method for preparing the starch-acrylic acid graft copolymer is different, as follows:
[0074] (1) Preparation of starch-acrylic acid graft copolymer
[0075] S1: Add 18kg cornstarch to 80kg water and mix evenly, then heat up to 55°C, reflux and stir for 40min to obtain starch solution A;
[0076] S2: Add 12kg of cornstarch into 40kg of water and mix evenly, then cool down to 10°C, stir and react for 1 hour to obtain starch solution B;
[0077] S3: After uniformly mixing the starch solution A and the starch solution B, a mixture A is obtained;
[0078] S4: Add 0.05kg of initiator and 0.4kg of crosslinking agent to 40kg of methacrylic acid solution with a mass concentration of 20%, stir until dissolved and mix uniformly to obtain mixture B; wherein, the initiator of this embodiment uses potassium persulfate , the crosslinking agent is 1,4-butanediol ester;
[0079] S5: Under the prot...
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