Fireproof composition and preparation method and application thereof
A technology of composition and mixture, which is applied in the field of materials, can solve the problems of energy crisis and fireproof materials without self-cooling function, and achieve the effects of improving air permeability, increasing porosity, and increasing moisture transfer rate
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[0042] The preparation method includes: adding phenol into the reaction vessel, adding part of formaldehyde, dicyandiamide and part of the catalyst at a speed of 800r / min to 1000r / min, then raising the temperature to 65°C to 75°C within 30min, and keeping it warm for 10min to 20min;
[0043] Raise the temperature to 80°C-100°C within 40min, keep it warm for 15min-25min, then cool down to 60°C-65°C, and then add the remaining amount of formaldehyde, the remaining amount of catalyst and water;
[0044] Raise the temperature to 80℃~100℃ within 20min, and maintain the viscosity at 3000mpa·s~5000mpa·s;
[0045] Add 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide and an ether solvent, heat to 110°C-130°C, keep it warm for 1.5h-2.5h, and then cool down to room temperature.
[0046] Within the range of preset mass parts, formaldehyde, phenol and dicyandiamide can react to generate dicyandiamide phenolic resin, and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) passes It...
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