Pasty organic peroxide cross-linking agent and compounding process thereof
An organic peroxide and cross-linking agent technology, which is applied in the field of pasty organic peroxide cross-linking agent and its compounding process, can solve the problems of poor product uniformity, unstable system, uneven dispersion, etc., and achieve convenient Transportation and use, excellent physical stability, excellent effect of physical stability
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Embodiment 1
[0029] A compounding process of a pasty organic peroxide type crosslinking agent, comprising the following steps:
[0030] Step 1, mix dibenzoyl peroxide and water according to the ratio of 47% to 53% by weight of dibenzoyl peroxide and 14% to 18% of water to prepare dibenzoyl peroxide and water mixture, spare;
[0031] Step 2: Add 20% to 24% phlegmatizer by weight to the mixture of dibenzoyl peroxide and water in step 1, turn on the stirring device, and stir for 0.5h to 1.0h at a speed of 2000r / min to 2500r / min , stir evenly, make the mixture of dibenzoyl peroxide, water and phlegmatizer, set aside;
[0032] Step 3, add 0.1% to 2.0% of nonionic surfactant and 4% to 15% of inorganic filler by weight into the mixture of dibenzoyl peroxide, water and phlegmatizer in step 2, and start the emulsifier for emulsification , continue for 1.0h to 3.0h to obtain an emulsion;
[0033] Step 4: add a phlegmatizer to the emulsified product in step 3 by weight, so that the phlegmatizer is...
Embodiment 2
[0039] A compounding process of a pasty organic peroxide type crosslinking agent, comprising the following steps:
[0040] Step 1, mix dibenzoyl peroxide and water according to the ratio of 47% to 53% by weight of dibenzoyl peroxide and 14% to 18% of water to prepare dibenzoyl peroxide and water mixture, spare;
[0041] Step 2, adding 20% to 26% of phlegmatizer by weight to the mixture of dibenzoyl peroxide and water in step 1, stirring evenly to make a mixture of dibenzoyl peroxide, water and phlegmatizer, spare;
[0042] Step 3, adding 0.1% to 2.0% of nonionic surfactant and 4% to 15% of inorganic filler by weight into the mixture of dibenzoyl peroxide, water and phlegmatizer in step 2, and emulsifying to obtain Paste organic peroxide crosslinking agent.
[0043] During compounding, turn on the temperature control device and keep the system temperature at 20°C to 25°C.
[0044] The above-mentioned nonionic surfactant refers to a polyether type nonionic surfactant, whic...
Embodiment 3
[0048] A compounding process of a pasty organic peroxide type crosslinking agent, comprising the following steps:
[0049] Step 1, the dibenzoyl peroxide and water are mixed in advance, the content of dibenzoyl peroxide is 75% (by weight), and the others are moisture to make a mixture of dibenzoyl peroxide and water, spare;
[0050]Step 2, in the 5L enamel reactor that common emulsifying machine, agitator are equipped with, add 2680g dibenzoyl peroxide and water mixture (water content rate 25%), 920g acetyl tributyl citrate in step 1, Turn on the stirring device, according to the rotating speed of 2200r / min, stir for 0.6h, stir evenly, make a mixture of dibenzoyl peroxide, water and acetyl tributyl citrate, set aside;
[0051] Step 3, add 80g polyether type nonionic surfactant PluronicRPE, 240g nano-calcium carbonate by weight in the mixture of dibenzoyl peroxide, water and acetyl tributyl citrate in step 2, open the emulsifier and emulsify , continued for 2.0h to obtain an ...
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