A kind of antibacterial application of dehydromethrin c
A technology for dehydromethrin and its use, which is applied in the field of medicine, can solve problems such as unseen literature or patent reports, and achieve the effects of simple separation and purification, improved survival rate, high yield and purity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment Construction
[0055] The present invention will be described in further detail below in conjunction with the accompanying drawings and embodiments. The examples are only used to explain the present invention, not to limit the protection scope of the present invention.
[0056] (1) Preparation of isoguaialide C ( figure 1 )
[0057] a) In a 250mL double-necked flask, add dehydrocoylolide (3.0g, 13.0mmol), SeO 2 (0.723g, 6.5mmol) and tert-butanol peroxide (3.6mL, 26.0mmol), and then 150mL of dichloromethane was added to obtain a reaction mixture. The reaction mixture was stirred at room temperature for 2h, and the reaction was monitored by TLC.
[0058] b) After the reaction finishes, the reaction product is washed with 10mL saturated Na 2 SO 3 The solution was washed twice to remove excess tert-butanol peroxide, and the organic phase was washed once with 10mL saturated sodium bicarbonate solution and saturated brine respectively, and then washed with anhydrous Na 2 SO 4 After drying, d...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 


