Integrated black silica gel OCR for improving performance based on crosslinking density and preparation method ofintegrated black silica gel OCR
A technology for improving performance and cross-linking density, applied in the field of polymer nano-organosilicon materials, can solve the problems of decreased OCR mechanical ability of silica gel, affecting product quality, and difficulty in improving one-piece black
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Embodiment 1
[0027] Embodiment 1 The one-piece black silica gel OCR and its preparation method based on cross-linking density to improve performance, including:
[0028] 1. Preparation of component A
[0029] Take 95% of divinyl polydimethylsiloxane, add it to a double-helix conical mixer, then add 5% platinum catalyst, and mix well to prepare component A;
[0030] 2. Preparation of component B
[0031] Take 80% of divinyl polydimethylsiloxane and 1% of cross-linking agent, add it to the double-helix conical mixer, then add 1% of accelerator, after mixing evenly, add coloring to component B in batches Add 0.01% of the agent, and stir evenly to prepare translucent B component;
[0032] 3. Preparation of addition-type thermally conductive silicone gel
[0033] Put component A and component B at a mass ratio of 1:1, add them to a double-helix conical mixer, and mix to obtain silica gel. Put the silica gel in a vacuum drying oven for 5-20 minutes to defoam, and pour the rubber into For the...
Embodiment 2
[0034] Embodiment 2 The one-piece black silica gel OCR and its preparation method based on cross-linking density to improve performance, including:
[0035] 1. Preparation of component A
[0036] Take 90% of divinyl polydimethylsiloxane, add it to a double-helix conical mixer, then add 4% platinum catalyst, and mix well to prepare component A;
[0037] 2. Preparation of component B
[0038] Take 82% of divinyl polydimethylsiloxane and 5% of cross-linking agent, add them to the double-helix conical mixer, then add accelerator 2, after mixing evenly, add the coloring agent to component B in batches 2%, and stir evenly to obtain translucent B component;
[0039] 3. Preparation of addition-type thermally conductive silicone gel
[0040] Put component A and component B at a mass ratio of 1:1, add them to a double-helix conical mixer, and mix to obtain silica gel. Put the silica gel in a vacuum drying oven for 5-20 minutes to defoam, and pour the rubber into For the mold, the te...
Embodiment 3
[0041] Embodiment 3 The one-piece black silica gel OCR and its preparation method based on cross-linking density to improve performance, including:
[0042] 1. Preparation of component A
[0043] Take 85% of divinyl polydimethylsiloxane, add it to a double-helix conical mixer, then add 3% platinum catalyst, and mix well to prepare component A;
[0044] 2. Preparation of component B
[0045] Take 85% of divinyl polydimethylsiloxane and 10% of cross-linking agent, add it to the double-helix conical mixer, then add 3% of accelerator, after mixing evenly, add coloring to component B in batches Add 3% of the agent, and stir evenly, so as to prepare the translucent B component;
[0046] 3. Preparation of addition-type thermally conductive silicone gel
[0047] Put component A and component B at a mass ratio of 1:1, add them to a double-helix conical mixer, and mix to obtain silica gel. Put the silica gel in a vacuum drying oven for 5-20 minutes to defoam, and pour the rubber into...
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